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EN
Mica glass-ceramic was prepared by sintering method from in the SiO_2-Al_2O_3-MgO-K_2O-B_2O_3-F_2 system. The sintering behavior and machinability of a glass-ceramic composition were examined. The starting materials were mixed and milled in an alumina ball mill for 2 h. Then the powders were sieved to obtain grain sizes smaller than 75 μm. For the shaping process, disc samples were prepared by pressing at 100 MPa. The pressed discs were sintered at temperatures in the range from 900 to 1200C for 2 h in an electric furnace using a heating rate of 5°C/min. X-ray diffraction analysis, scanning electron microscopy, and machinability tests for characterization were performed on sintered samples. The results showed that all samples exhibited similar phases formation and good machinability.
EN
In this study, the effect of impact angle of the particles on solid particle erosive wear properties of basalt base glass-ceramics used for industrial applications was investigated. Commercial basalt glass-ceramic materials size of 20×20×3 cm was sectioned to the size of 5×5×1.2 cm. The experimental procedure was performed by using erosive wear test device with nozzle diameter of 0.78 cm. Na feldspar size of 300 μm was used as erosive media. The samples were fixed 2 cm distance from the nozzle, Na feldspar particles were sprayed by using 1.5, 3, 4 bar pressure for 20 s. The tests were repeated with 30°+45°+60°+75°+90° impact angles. The erosive wear rates were measured and the effect of particle impact angle on wear properties was determined.
EN
In this study, machinable glass-ceramics were produced from vermiculite and K₂CO₃, SiO₂, Al₂O₃ and MgF₂ as additives by melting process. The starting materials were mixed together and milled in a mill with alumina ball for 2 h. The mixed powders were melted by aluminum crucible at 1500°C. The melted glass was cast into graphite mold, and then it was exposed to crystallization heat treatment for glass-ceramic transformation. The glass-ceramic samples were characterized with X-ray diffraction analysis, scanning electron microscopy, mechanical tests such as hardness, fracture toughness and machinability test. The results indicate that machinability properties can be obtained from vermiculite based glass-ceramic with some additives.
EN
Glass-ceramics were produced by sintering method from industrial waste materials such as fly ash, blast furnace slag and boron waste. The sintering behavior and machinability of glass-ceramic compositions were investigated. Additives were added to waste materials for enhancement of machinability and sintering properties. All starting materials were mixed by ball milling for 2 h using alumina media. The mixed and milled powders were sieved to grain sizes smaller than 75 μm and pressed at 100 MPa. The pressed samples were sintered at 900°C, 1000°C and 1100°C for 1 h in an electric furnace using a heating rate of 5°C/min. Some characterization tests such as X-ray diffraction (XRD), scanning electron microscopy (SEM) and machinability tests were performed on sintered samples. The results indicated that all samples exhibit good sintering and machinability properties.
EN
In this study, the effects of perlite addition on mechanical properties and wear resistance of alumina ceramics were investigated. Alumina powders including perlite 5%, 10%, 15%, 20% and perlite free were prepared. These powders were shaped as rectangular by using uniaxial pressing system under the load of 100 MPa. The samples were sintered at 1400°C-1550C for 2 h and were subjected to some mechanical tests such as hardness and fracture toughness. X-ray diffraction analysis was employed to determine the crystalline phases. Bulk densities of the samples were measured. In addition, erosive wear test was performed to investigate the erosive wear resistance of the samples. The wear test results were presented depending on different sliding speed and sintering temperature. These results showed that perlite addition has a positive effect on erosive wear resistance of the alumina ceramics, generally.
6
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Bond Strength of Basalt Based Glass-Ceramic Coatings

81%
EN
In the present study, powders produced from the volcanic basalt rocks were coated on pre-coated AISI 1040 steel with Ni-5% Al bond coat by atmospheric plasma spray coating technique. The coated specimens were characterized by optical microscopy, scanning electron microscopy, metallography and X-ray diffraction. Bonding strength of coatings was evaluated in accordance with the ASTM C-633 method. Coated basalt material from the APS coating system was determined in the glassy amorphous state by X-ray diffraction analysis. The coated samples were heat-treated at 800C for 1-4 h for crystallization. The phases formed in the basalt base glass-ceramic coatings were augite, Fe-diopside, anorthite, and andesine which were detected by X-ray diffraction analysis. Basalt based glass-ceramic coatings include splat, porosity and un-melted particles which were the characteristic of plasma sprayed coatings. Experiment result showed that the crystallization time increase caused the decrease of the bond strengths of the coatings.
7
81%
EN
In the current study, the effect of boron waste addition on some properties of fly ash based glass and glass-ceramics were investigated. The powder compositions including 10, 30, and 50 wt% boron waste was prepared. All the investigated compositions were melted at 1500C by using electrical furnaces. Melting structures were cast into the graphite mold. Thus, fly ash-boron waste based glass materials were produced. To transform the glass-ceramic, crystallization process was performed. Crystallization and glass-transition temperatures were determined by differential thermal analysis. Highly dense and crystalline materials, predominantly composed of diopside and augite together with tincalconite and residual glassy phase, were detected by X-ray diffraction analysis after heat treatment at 800, 900, and 1000C for 1 h. For the glass and glass-ceramic samples, mechanical tests such as hardness and fracture toughness were realized. A boron waste addition has a positive effect on the hardness of the specimens unlike the fracture toughness results. Furthermore, produced glass-ceramic materials were characterized via scanning electron microscopy.
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