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Journal
2013 | 11 | 8 | 1343-1351
Article title

Determination of some frequently used antibiotics in waste waters using solid phase extraction followed by high performance liquid chromatography with diode array and mass spectrometry detection

Content
Title variants
Languages of publication
EN
Abstracts
EN
This study is focused on the determination of some important antibiotics from different classes in waste water samples using solid phase extraction followed by high performance liquid chromatography with two detectors, diode array and mass spectrometer in positive ionisation mode. The investigated antibiotics include three penicillins (amoxicillin, ampicillin, penicillin G), two cephalosporins (ceftazidime, ceftriaxone), and two tetracyclines (tetracycline, doxycycline). The studied antibiotics were extracted from waste water samples using hydrophilic-lipophilic balanced cartridges. The extraction of antibiotics from water matrices was tested at several pH values. The best recoveries were obtained at pH 3 and 7 respectively. Depending on the nature of antibiotic, the limits of detection and quantification were obtained in the range of 0.07–0.92 µg mL−1 and 0.21–2.77 µg mL−1 respectively. Influent and effluent waste water samples were collected from a Waste Water Treatment Plant from Romania in order to detect the studied antibiotics. The antibiotics detected in the influent waste water samples were ceftriaxone (334 µg L−1), tetracycline (146 µg L−1) and doxycycline (110 µg L−1). In effluent waste water samples no target antibiotics were detected. [...]
Publisher

Journal
Year
Volume
11
Issue
8
Pages
1343-1351
Physical description
Dates
published
1 - 8 - 2013
online
1 - 6 - 2013
Contributors
author
  • National Institute for Research and Development of Isotopic and Molecular Technologies, Cluj-Napoca, 400293, Romania
  • National Institute for Research and Development of Isotopic and Molecular Technologies, Cluj-Napoca, 400293, Romania, loredana.soran@itim-cj.ro
  • “Raluca Ripan“ Institute for Research in Chemistry, Babeş-Bolyai University, Cluj-Napoca, 400294, Romania
  • “Raluca Ripan“ Institute for Research in Chemistry, Babeş-Bolyai University, Cluj-Napoca, 400294, Romania
  • Faculty of Environmental Sciences and Engineering, Babeş-Bolyai University, Cluj-Napoca, 400294, Romania
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Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-013-0263-y
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