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2013 | 11 | 5 | 736-741
Article title

Sensitive and fast determination of papaverine by adsorptive stripping voltammetry on renewable mercury film electrode

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EN
Abstracts
EN
The renewable mercury film electrode, applied for the determination of papaverine traces using differential pulse adsorptive stripping voltammetry (DP AdSV) is presented. The calibration graph obtained for papaverine is linear from 1.25 nM (0.42 µg L−1) to 95 nM (32.2 µg L−1) for a preconcentration time of 60 s, with correlation coefficient of 0.998. For the renewable mercury electrode (Hg(Ag)FE) with a surface area of 9.1 mm2 the detection limit for a preconcentration time of 60 s is 0.7 nM (0.24 µg L−1). The repeatability of the method at a concentration level of the analyte as low as 17 µg L−1, expressed as RSD is 3.3% (n=5). The proposed method was successfully applied and validated by studying the recovery of papaverine from drugs, urine and synthetic solution. [...]
Publisher
Journal
Year
Volume
11
Issue
5
Pages
736-741
Physical description
Dates
published
1 - 5 - 2013
online
27 - 2 - 2013
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Document Type
Publication order reference
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-013-0208-5
Identifiers
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