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Number of results

Journal

2013 | 11 | 5 | 736-741

Article title

Sensitive and fast determination of papaverine by adsorptive stripping voltammetry on renewable mercury film electrode

Content

Title variants

Languages of publication

EN

Abstracts

EN
The renewable mercury film electrode, applied for the determination of papaverine traces using differential pulse adsorptive stripping voltammetry (DP AdSV) is presented. The calibration graph obtained for papaverine is linear from 1.25 nM (0.42 µg L−1) to 95 nM (32.2 µg L−1) for a preconcentration time of 60 s, with correlation coefficient of 0.998. For the renewable mercury electrode (Hg(Ag)FE) with a surface area of 9.1 mm2 the detection limit for a preconcentration time of 60 s is 0.7 nM (0.24 µg L−1). The repeatability of the method at a concentration level of the analyte as low as 17 µg L−1, expressed as RSD is 3.3% (n=5). The proposed method was successfully applied and validated by studying the recovery of papaverine from drugs, urine and synthetic solution. [...]

Publisher

Journal

Year

Volume

11

Issue

5

Pages

736-741

Physical description

Dates

published
1 - 5 - 2013
online
27 - 2 - 2013

Contributors

author
  • Faculty of Materials Science and Ceramics, AGH University of Science and Technology, 30-059, Kraków, Poland
  • Faculty of Materials Science and Ceramics, AGH University of Science and Technology, 30-059, Kraków, Poland

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-013-0208-5
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