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2012 | 10 | 4 | 1310-1317
Article title

Voltammetric and amperometric determination of metoclopramide on boron-doped diamond film electrode

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EN
Abstracts
EN
New methods for the determination of metoclopramide, antiemetic and gastroprokinetic pharmaceutical, were developed, using differential pulse voltammetry (DPV) and flow injection analysis (FIA) with amperometric detection on a boron-doped diamond film electrode. Electrode pretreatment necessary to ensure the stable results was investigated and it was found, that while DPV requires frequent electrode cleaning, FIA with a sufficiently high flow rate can maintain a stable signal with no signs of electrode passivation. The calculated quantification limits of the DPV and FIA with amperometric detection were 0.13 μmol L−1 and 0.015 mmol L−1, respectively. The applicability of the new methods was verified by the determination of metoclopramide in a pharmaceutical preparation. FIA with amperometic detection proved to be sensitive, accurate and, due to the resistance of the electrode to the passivation, also simple to handle. [...]
Publisher

Journal
Year
Volume
10
Issue
4
Pages
1310-1317
Physical description
Dates
published
1 - 8 - 2012
online
29 - 5 - 2012
Contributors
author
  • UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Faculty of Science, Charles University in Prague, CZ-12843, Prague 2, Czech Republic, dejmkova@natur.cuni.cz
author
  • Department of Chemistry, Faculty of Science, Anadolu University, 26470, Eskisehir, Turkey
author
  • UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Faculty of Science, Charles University in Prague, CZ-12843, Prague 2, Czech Republic
author
  • UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Faculty of Science, Charles University in Prague, CZ-12843, Prague 2, Czech Republic
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Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-012-0056-8
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