Voltammetric and amperometric determination of metoclopramide on boron-doped diamond film electrode

• Authors: Hana Dejmkova , Candan Dag , Jiri Barek , Jiri Zima
• Languages of publication: EN

Abstracts

EN

New methods for the determination of metoclopramide, antiemetic and gastroprokinetic pharmaceutical, were developed, using differential pulse voltammetry (DPV) and flow injection analysis (FIA) with amperometric detection on a boron-doped diamond film electrode. Electrode pretreatment necessary to ensure the stable results was investigated and it was found, that while DPV requires frequent electrode cleaning, FIA with a sufficiently high flow rate can maintain a stable signal with no signs of electrode passivation. The calculated quantification limits of the DPV and FIA with amperometric detection were 0.13 μmol L−1 and 0.015 mmol L−1, respectively. The applicability of the new methods was verified by the determination of metoclopramide in a pharmaceutical preparation. FIA with amperometic detection proved to be sensitive, accurate and, due to the resistance of the electrode to the passivation, also simple to handle. [...]

Keywords

EN

Metoclopramide; Differential pulse voltammetry; Flow injection analysis; Boron-doped diamond film electrode; Passivation

• Publisher: De Gruyter Open
• Journal: Open Chemistry
• Year: 2012
• Volume: 10
• Issue: 4
• Pages: 1310-1317

Dates

published

1 - 8 - 2012

online

29 - 5 - 2012

Contributors

author

Hana Dejmkova

• UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Faculty of Science, Charles University in Prague, CZ-12843, Prague 2, Czech Republic

author

Candan Dag

• Department of Chemistry, Faculty of Science, Anadolu University, 26470, Eskisehir, Turkey

author

Jiri Barek

• UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Faculty of Science, Charles University in Prague, CZ-12843, Prague 2, Czech Republic

author

Jiri Zima

• UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Faculty of Science, Charles University in Prague, CZ-12843, Prague 2, Czech Republic

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Identifiers

DOI

10.2478/s11532-012-0056-8