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Number of results

Journal

2011 | 9 | 3 | 453-459

Article title

Self-assembled hydrogen-bonded coordination networks in two copper(II) carboxylates with 4-pyridylmethanol

Content

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Languages of publication

EN

Abstracts

EN
The crystal and molecular structure of [Cu(nif)2(4-PM)2]·CH3OH (1) and [Cu(2-Clbz)2(4-PM)2(H2O)] (2), (where nif = niflumate anion, 2-Clbz = 2-chlorobenzoate anion and 4-PM is the 4-pyridylmethanol), have been determinated by X-ray crystallography. The Cu2+ cation in (1), is coordinated by two pairs of oxygen atoms from asymmetric bidentate niflumate anions and by a pair of pyridine nitrogen atoms from monodentate 4-pyridylmethanol ligands in trans position forming an extremely elongated bipyramid. The Cu2+ cation in (2), is coordinated by a pair of oxygen atoms from monodentate 2-chlorobenzoate anions, further by a pair of pyridine nitrogen atoms from monodentate 4-pyridylmethanol ligands and finally by a water oxygen atom forming a tetragonal-pyramidal coordination polyhedron. The molecules of both complexes in crystal structures are linked by O-H…O hydrogen bonds, which created a three-dimensional hydrogen-bonding networks. The Π-Π stacking interactions are also observed in crystal structures of complex 2. The spectral properties (IR and electronic spectra) of both complexes were also investigated.

Publisher

Journal

Year

Volume

9

Issue

3

Pages

453-459

Physical description

Dates

published
1 - 6 - 2011
online
22 - 3 - 2011

Contributors

  • Slovak University of Technology
author
  • Slovak University of Technology
  • University of Pardubice
  • University of Jyväskylä
author
  • University of Wroclaw
author
  • Slovak University of Technology

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-011-0023-9
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