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2015 | 60 | 1 | 87-91
Article title

The influence of thermal annealing on structure and oxidation of iron nanowires

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Raman spectroscopy as well as Mössbauer spectroscopy were applied in order to study the phase composition of iron nanowires and its changes, caused by annealing in a neutral atmosphere at several temperatures ranging from 200°C to 800°C. As-prepared nanowires were manufactured via a simple chemical reduction in an external magnetic field. Both experimental techniques proved formation of the surface layer covered by crystalline iron oxides, with phase composition dependent on the annealing temperature (Ta). At higher Ta, hematite was the dominant phase in the nanowires.
Physical description
1 - 3 - 2015
12 - 3 - 2015
18 - 6 - 2014
2 - 11 - 2014
  • 1. Chertok, B., Moffat, B. A., David, A. E., Yu, F., Bergemann, C., Ross, B. D., & Yang, V. C. (2008). Iron oxide nanoparticles as a drug delivery vehicle for MRI monitored magnetic targeting of brain tumors. Biomaterials, 29(4), 487–496. DOI: 10.1016/j.biomaterials.2007.08.050.[Crossref][PubMed]
  • 2. Zhang, X. X., Wen, G. H., Huang, S., Dai, L., Gao, R., & Wang, Z. L. (2001). Magnetic properties of Fe nanoparticles trapped at the tips of the aligned carbon nanotubes. J. Magn. Magn. Mater., 231(1), 9–12. DOI: 10.1016/S0304-8853(01)00134-2.[Crossref]
  • 3. Bolm, C., Legros, J., Le Paih, J., & Zani, L. (2004). Iron-catalyzed reactions in organic synthesis. Chem. Rev., 104(12), 6217–6254. DOI: 10.1021/cr040664h.[Crossref]
  • 4. Getzlaff, M., Bansmann, J., & Schonhense, G. (1995). Oxygen on Fe(100) and Fe(110). Fresenius J. Anal. Chem., 353(5/8), 743–747. DOI: 10.1007/BF00321362.[Crossref]
  • 5. Zeeshan, M. A., Pane, S., Youn, S. K., Pellicer, E., Schuerle, S., Sort, J., Fusco, S., Lindo, A. M., Park, H. G., & Nelson, B. J. (2013). Graphite coating of iron nanowires for nanorobotic applications: Synthesis, characterization and magnetic wireless manipulation. Adv. Funct. Mater., 23(7), 823–831. DOI: 10.1002/adfm.201202046.[Crossref]
  • 6. Lin, W. S., Jian, Z. J., Lin, H. M., Lai, L. C., Chiou, W. A., Hwu, Y. K., Wu, S. H., Chen, W. C., & Yao, Y. D. (2013). Synthesis and characterization of iron nanowires. J. Chinese Chem. Soc., 60(1), 85–91. DOI: 10.1002/jccs.201200263.[Crossref]
  • 7. Jubb, A. M., & Allen, H. C. (2010). Vibrational spectroscopic characterization of hematite, maghemite, and magnetite thin films produced by vapor deposition. ACS Appl. Mater. Interfaces, 2(10), 2804–2812. DOI: 10.1021/am1004943.[Crossref][WoS]
  • 8. Cornell, R. M., & Schwertmann, U. (2003). The iron oxides. Structure, properties, reactions, occurrences and uses. Weinheim, Germany: Wiley-VCH.
  • 9. Wang, C. M., Baer, D. R., Amonette, J. E., Engelhard, M. H., Antony, J., & Qiang, Y. (2009). Morphology and electronic structure of the oxide shell on the surface of iron nanoparticles. J. Am. Chem. Soc., 131(25), 8824–8832. DOI: 10.1021/ja900353f.[Crossref]
  • 10. Long, G. J., Hautot, D., Pankhurst, Q. A., Vandormael, D., Grandjean, F., Gaspard, J. P., Briois, V., Hyeon, T., & Suslick, K. S. (1998). Mossbauer-Bauer-effect and x-ray-absorption spectral study of sonochemically prepared amorphous iron. Phys. Rev. B, 57(17), 10716–10722. DOI: 10.1103/PhysRevB.57.10716.[Crossref]
  • 11. Machala, L., Zboril, R., & Gedanken, A. (2007). Amorphous iron(III) oxide – a review. J. Phys. Chem. B, 111(16), 4003–4018. DOI: 10.1021/jp064992s.[Crossref]
  • 12. Cao, X., Koltypin, Y., Katabi, G., & Prozorov, R. (1997). Preparation and characterization of amorphous nanometre sized Fe3O4 powder. J. Mater. Chem., 7(6), 1007–1009. DOI: 10.1039/a606739e.[Crossref]
  • 13. Petrov, Y. I., & Shafranovsky, E. A. (2012). On the conditions eliciting a detailed structure in the hyperfine field distribution at 57Fe nuclei. Nucl. Instrum. Methods Phys. Res. Sect. B-Beam Interact. Mater. Atoms, 271, 96–101. DOI: 10.1016/j.nimb.2011.10.014.[Crossref]
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