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Number of results
2014 | 126 | 4 | 938-942

Article title

Comparative Study of Phases Forming in Niobium-Antimony Oxides System upon High Temperature Treatment and High-Energy Ball Milling

Content

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EN

Abstracts

EN
The compound SbNbO_4 that is formed in a ternary system of Nb-Sb-O has been obtained for the first time by high-energy ball milling of the equimolar mixture of oxides Sb_2O_3/Nb_2O_5in argon atmosphere. This compound was characterised by X-ray diffraction, differential thermal analysis- thermal gravimetry, infrared, and scanning electron microscopy methods and its properties were compared with those of SbNbO_4 also obtained as a result of high-temperature reaction between the same oxides and also in argon atmosphere. As shown by differential thermal analysis results, irrespective of the method of synthesis, SbNbO_4 is stable in argon atmosphere up to ≈ 1125°C and in air up to ≈ 800°C. The compound can be applied as a photocatalyst in the reaction of producing hydrogen from water.

Keywords

EN

Contributors

author
  • Cracow University of Technology, Faculty of Chemical Engineering and Technology, Warszawska 24, 31-155 Kraków, Poland
author
  • West Pomeranian University of Technology Szczecin, Faculty of Technology and Chemical Engineering, al. Piastów 42, 71-065 Szczecin, Poland
author
  • West Pomeranian University of Technology Szczecin, Faculty of Technology and Chemical Engineering, al. Piastów 42, 71-065 Szczecin, Poland
  • Cracow University of Technology, Faculty of Chemical Engineering and Technology, Warszawska 24, 31-155 Kraków, Poland

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.bwnjournal-article-appv126n416kz
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