Time Resolved IR and X-Ray Simultaneous Spectroscopy: New Opportunities for the Analysis of Fast Chemical-Physical Phenomena in Materials Science

• Authors: A. Marcelli , D. Hampai , Wei Xu , L. Malfatti , P. Innocenzi
• Languages of publication: EN

Abstracts

EN

New powerful sources and advanced analytical techniques have been considered in the last decade to face up the continuously increasing scientific demands, in particular, in materials science. As an example, nano- science and nanotechnology researches are characterized by ultimate spatial resolution, fast and ultrafast time-resolved analysis, but the complexity of the investigated phenomena requires new analytical capabilities and new experimental techniques were introduced in the research arena. The availability all over the world of brilliant synchrotron radiation sources offers incredible opportunities. Many challenging experiments were made possible by these sources and understanding of many complex dynamical problems was obtained. Nevertheless, a strong demand of new analytical approaches, mainly based on concurrent and possibly simultaneous time-resolved experimental techniques, is emerging. Pioneering time resolved experiments combining X-ray and infrared radiation with a conventional source were performed more than a decade ago. Nowadays, many beamlines at third generation synchrotron radiation facilities are equipped with conventional sources to allow complementary techniques and the strategy of a concurrent analysis is mandatory in the investigation of many phenomena in frontier multidisciplinary researches. Moreover, new opportunities will be available by means of concurrent spectroscopic experiments investigating complex phenomena on a short timescale, from the sub-second to the microsecond time domain. We will present and discuss researches where the combination of IR and X-ray simultaneous experiments may return unique information on complex dynamical processes and phase transitions occurring in materials science. Finally, we will briefly describe the conceptual layout of a synchrotron radiation beamline to perform concurrent IR and X-ray experiments.

Keywords

EN

07.85.Qe; 61.05.cj; 82.20.-w; 78.47.-p

Discipline

• 61.05.cj: X-ray absorption spectroscopy: EXAFS, NEXAFS, XANES, etc.(for x-ray and EXAFS applications in biological physics, see 87.64.kd)
• 82.20.-w: Chemical kinetics and dynamics
• 07.85.Qe: Synchrotron radiation instrumentation
• 78.47.-p: Spectroscopy of solid state dynamics

• Publisher: Institute of Physics, Polish Academy of Sciences
• Journal: Acta Physica Polonica A
• Year: 2009
• Volume: 115
• Issue: 2
• Pages: 489-500

Dates

published

2009-02

Contributors

author

A. Marcelli

• Laboratori Nazionali di Frascati - INFN, Via E. Fermi 40, 00044 Frascati, Rome, Italy

author

D. Hampai

• Laboratori Nazionali di Frascati - INFN, Via E. Fermi 40, 00044 Frascati, Rome, Italy

author

Wei Xu

• Laboratori Nazionali di Frascati - INFN, Via E. Fermi 40, 00044 Frascati, Rome, Italy
• Institute of High Energy Physics, Chinese Academy of Science, Beijing 100049, China

author

L. Malfatti

• Laboratorio di Scienza dei Materiali e Nanotecnologie, Università di Sassari D.A.P., CR-INSTM, Palazzo Pou Salit, Piazza Duomo 6, 07041 Alghero, Sassari, Italy

author

P. Innocenzi

• Laboratorio di Scienza dei Materiali e Nanotecnologie, Università di Sassari D.A.P., CR-INSTM, Palazzo Pou Salit, Piazza Duomo 6, 07041 Alghero, Sassari, Italy

References

• 1. P. Innocenzi, L. Malfatti, T. Kidchob, S. Costacurta, P. Falcaro, M. Piccinini, A. Marcelli, P. Morini, D. Sali, H. Amenitsch, J. Phys. Chem. C 111, 5345 (2007)
• 2. W. Bras, G.E. Derbyshire, D. Bogg, J. Cooke, M.J. Elwell, B.U. Komanschek, S. Naylor, A.J. Ryan, Science 267, 996 (1995)
• 3. M.A. Newton, A.J. Dent, S.G. Fiddy, B. Jyotid, J. Evans, Phys. Chem. Chem. Phys. 9, 246 (2007)
• 4. R.J. Davies, M. Burghammer, C. Riekel, Macromolecules 39, 4834 (2006)
• 5. M.A. Newton, A.J. Dent, S.G. Fiddy, B. Jyoti, J. Evans, Catalysis Today 126, 64 (2007)
• 6. B.S. Clausen, H. Topsοe, R. Frahm, Adv. Catal. 42, 315 (1998)
• 7. G.S. Sankar, J.M. Thomas, Top. Catal. 8, 1 (1999)
• 8. J.G. Mesu, A.M.J. van der Eerden, F.M.F. de Groot, B.M. Weckhuysen, J. Phys. Chem. B 109, 4042 (2005)
• 9. S. Diaz-Moreno, D.T. Bowron, J. Evans, Dalton Trans. 23, 3814 (2005)
• 10. G. Guilera, M.A. Newton, C. Polli, S. Pascarelli, M. Guino, K.K. Hii, Chem. Commun. 41, 4306 (2006)
• 11. A.M. Beale, A.M.J. van der Eerden, K. Kervinen, M.A. Newton, B.M. Weckhuysen, Chem. Commun. 24, 3015 (2005)
• 12. V. Briois, D. Lutzenkirchen-Hecht, F. Villain, E. Fonda, S. Belin, B. Griesebock, R. Frahm, J. Phys. Chem. A 109, 320 (2005)
• 13. J.D. Grunwald, M. Ramin, M. Rohr, A. Michailovski, G.R. Patzke, A. Baiker, Rev. Sci. Instrum. B 76, 054104 (2005)
• 14. X-ray Absorption: Principles, Applications, Techniques of EXAFS, SEXAFS, XANES, Eds. D.C. Konigsberger, R. Prins, Wiley, New York 1988
• 15. R. Phillips, S.R. Quake, Phys. Today 59, 38 (2006)
• 16. N.A. Young, J. Chem. Soc., Dalton Trans. 249, 96
• 17. O.M. Wilkin, N.A. Young, J. Synchrotron Rad. 6, 204 (1999)
• 18. M. Cestelli Guidi, M. Piccinini, A. Marcelli, A Nucara, P. Calvani, E. Burattini, J. Opt. Soc. Am. A 22, 2810 (2005)
• 19. C.J. Brinker, Y. Lu, A. Sellinger, H. Fan, Adv. Mater. 11, 579 (1999)
• 20. P. Innocenzi, T. Kidchob, L. Malfatti, S. Costacurta, M. Takahashi, M. Piccinini, A. Marcelli, J. Sol.-Gel. Sci. Technol. 48, 258 (2008)
• 21. G.D. Smith, R.A. Palmer, in: Handbook of Vibrational Spectroscopy, Eds. J.M. Chalmers, P.R. Griffiths, Wiley, Chichester 2002, Vol. 1, p. 626
• 22. P. Innocenzi, T. Kidchob, J. Mio Bertolo, M. Piccinini, M. Cestelli Guidi, A. Marcelli, J. Phys. Chem. B 110, 10837 (2006)
• 23. M. Antoietti, G.A. Ozin, Chem. Eur. J. 10, 28 (2004)
• 24. C.J. Brinker, D.R. Dunphy, Curr. Opin. Coll. Inter. Sci. 11, 126 (2006)
• 25. M. Takahashi, T. Maeda, K. Uemura, J. Yao, Y. Tokuda, Y. Yoko, Y. Kaji, A. Marcelli, P. Innocenzi, Adv. Mater. 19, 4343 (2007)
• 26. R. Peierls, Proc. Phys. Soc. London, Ser. A 49, 72 (1937)
• 27. M. Imada, A. Fujimori, Y. Tokura, Rev. Mod. Phys. 70, 1039 (1998)
• 28. A. Sacchetti, M. Cestelli Guidi, E. Arcangeletti, A. Nucara, P. Calvani, M. Piccinini, A. Marcelli, P. Postorino, Phys. Rev. Lett. 96, 035503 (2006)
• 29. S.-W. Cheong, H.Y. Hwang, in: Colossal Magnetoresistance Oxides, Ed. Y. Tokura, Monographs in Condensed Matter Science, Gordon and Breach, Reading, U.K. 2000, p. 237
• 30. A.J. Millis, B.I. Shraiman, R. Mueller, Phys. Rev. Lett. 77, 175 (1996)
• 31. A.J. Millis, Nature 392, 147 (1998)
• 32. W. Eberhardt, Surf. Sci. 500, 242 (2002)
• 33. H.W. Kroto, J.R. Heath, S.C. O'Brien, R.F. Curl, R.E. Smalley, Nature 318, 162 (1985)
• 34. J.R. Heath, S.C. O'Brien, Q. Zhang, Y. Lui, R.F. Curl, H.W. Kroto, R.E. Smalley, J. Am. Chem. Soc. 107, 7779 (1985)
• 35. D.S. Bethune, R.D. Johnson, J.R. Salem, M.S. de Veles, C.S. Yannoni, Nature 336, 123 (1993)
• 36. H. Shinohara, Rep. Prog. Phys. 63, 843 (2000)
• 37. J.R. Heflin, D. Marciu, C. Figura, S. Wang, P. Burbank, S. Stevenson, H.C. Dorn, Appl. Phys. Lett. 72, 2788 (1998)
• 38. M. Takata, E. Nishibori, M. Sakata, H. Shinohara, Struct. Bonding 109, 59 (2004)
• 39. L. Liu, B. Gao, W. Chu, D. Chen, T. Hu, C. Wang, L. Dunsch, A. Marcelli, Y. Luo, Z. Wu, Chem. Commun. 4, 474 (2008)
• 40. M.S. Dresselhaus, G. Dresselhaus, P.C. Eklund, Science of Fullerenes and Carbon Nanotubes, Academic Press, San Diego 1996
• 41. S. Guha, K. Nakamoto, Coord. Chem. Rev. 249, 1111 (2005)
• 42. A. Barth, C. Zscherp, Quart. Rev. Biophys. 35, 369 (2002)
• 43. D. Lützenkirchen-Hecht, S. Grundmann, R. Frahm, J. Synchrotron Rad. 8, 6 (2001)
• 44. M. Richwin, R. Zaeper, D. Lützenkirchen-Hecht, R. Frahm, Rev. Sci. Instrum. 73, 1668 (2002)
• 45. M. Haumann, M. Grabolle, M. Werthammer, L. Iuzzolino, J. Dittmer, W. Meyer-Klaucke, T. Neisius, H. Dau, PS2001 Proceedings, Contribution S10-013, p. 1 (2001)
• 46. M. Haumann, M. Grabolle, T. Neisius, H. Dau, FEBS Lett. 512, 116 (2002)
• 47. M. Haumann, P. Pospisil, M. Grabolle, C. Muéller, P. Liebisch, V.A. Sole', T. Neisius, J. Dittmer, H. Dau, J. Synchrotron Rad. 9, 304 (2002)
• 48. H. Dau, M. Haumann, J. Synchrotron Rad. 10, 76 (2003)
• 49. M. Haumann, C. Muller, P. Liebisch, T. Neisius, H. Dau, J. Synchrotron Rad. 12, 35 (2005)
• 50. O. Kleifeld, A. Frenkel, J.M.L. Martin, I. Sagi, Nature Struct. Biol. 10, 98 (2003)
• 51. J. Zhong, L. Song, J. Meng, B. Gao, W. Chu, H. Xu, Y. Luo, J. Guo, A. Marcelli, S. Xie, Z. Wu, Carbon 47, 967 (2009)
• 52. Xu Wei, Ph.D. Thesis, Graduate school of Chinese Academy of Sciences, Institute of High Energy Physics 2008
• 53. F. D'Acapito, F. Boscherini, A. Marcelli, S. Mobilio, Rev. Sci. Instrum. 63, 899 (1991)
• 54. M. Sánchez del Ríjo, R.J. Dejus, in: Synchrotron Radiation Instrumentation: Eighth Int. Conf., Eds. T. Warwick, J. Arthur, H.A. Padmore, J. Stöhr, American Institute of Physics, 2004, p. 784
• 55. R.O. Hettel, Rev. Sci. Instrum. 73, 1396 (2002)
• 56. M.F. Brigatti, D. Malferrari, M. Poppi, A. Mottana, G. Cibin, A. Marcelli, G. Cinque, Am. Mineral. 93, 821 (2008)
• 57. J. Headspith, J. Groves, P.N. Luke, M. Kogimtzis, G. Salvini, S.L. Thomas, R.C. Farrow, J. Evans, T. Rayment, J.S. Lee, W.D. Goward, M. Amman, O. Mathon, S. Diaz-Moreno, in: IEEE Nuclear Science Symp. Conf., Ed. M.W.T. Benjamin, IEEExplore 4, 2007, p. 2421
• 58. G.A. De Rose, H. Jiang, P.D. Holland, W.W. Adams, R.W. Hoffman, C.A. Zorman, Inter. Rep. Air Force Material Command (Ohio) Jan.-Sep. 1993, WL-TR-93-4107, p. 11
• 59. http://cars9.uchicago.edu/~newville/mcbook/
• 60. J.B. Hastings, in: Applications of EXAFS to Materials Science Conf., BNL-28946, http://www.osti.gov/bridge/product.biblio.jsp?osti_id=6862052
• 61. S. Pascarelli, O. Mathon, M. Munoz, T. Mairs, J. Susini, J. Synchrotron. Rad. 13, 351 (2006)
• 62. Workshop on Simultaneous Raman-X-ray Diffraction/Absorption Studies for the In Situ Investigation of Solid State Transformations and Reactions at Non Ambient Conditions, Grenoble 2008, at: http://www.esrf.eu/UsersAndScience/Experiments/CRG/BM01/raman_workshop/report

Identifiers

DOI

10.12693/APhysPolA.115.489