Application of the design of experiments in the epoxidation process of 1,5,9-cyclododecatriene

• Authors: Grzegorz Lewandowski , Jan Ćwirko
• Languages of publication: EN

Abstracts

EN

An influence of the molar ratio of cis, trans, trans-1,5,9-cyclododecatriene to tert-butyl hydroperoxide, the concentration of the catalyst and the reaction time on the performance of the epoxidation process of cis, trans, trans-1,5,9-cyclodecatriene with tert-butyl hydroperoxide at the presence of molybdenum hexacarbonyl Mo(CO)6 was examined. Examinations were performed using statistical methods of the design of experiments. A mathematical model describing the influence of the parameters on conversion cis, trans, trans-1,5,9-cyclododecatriene was obtained. An analysis of the data and rests was performed and an optimal value of conversion of cis, trans, trans-1,5,9-cyclododecatriene was established.

Keywords

EN

epoxidation; design of experiments; 1,5,9-cyclododecatriene; optimization

• Publisher: De Gruyter Open
• Journal: Polish Journal of Chemical Technology
• Year: 2007
• Volume: 9
• Issue: 4
• Pages: 68-71

Dates

published

1 - 12 - 2007

online

30 - 1 - 2008

Contributors

author

Grzegorz Lewandowski

• Institute of Organic Chemical Technology, Szczecin University of Technology, ul. Pułaskiego 10, 70-322 Szczecin, Poland

author

Jan Ćwirko

• Institute of Organic Chemical Technology, Szczecin University of Technology, ul. Pułaskiego 10, 70-322 Szczecin, Poland

References

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Identifiers

DOI

10.2478/v10026-007-0093-9