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Number of results

Journal

2014 | 12 | 12 | 1239-1245

Article title

Voltammetric behavior and quantitative determination of ambazone concentrations in urine and in a pharmaceutical formulation

Content

Title variants

Languages of publication

EN

Abstracts

EN
The use of square wave adsorptive stripping voltammetry (SWAdSV) in conjunction with a cyclic renewable silver amalgam film electrode (Hg(Ag)FE) for the analytical determination of ambazone in urine samples and pharmaceutical formulations is described. A single reduction peak in Britton-Robinson buffer at pH 4.0 was detected at about −1.4 V versus Ag/AgCl. Mechanistic studies have shown that the compound can act as an electrocatalyst. The method was validated. The analytical curve was linear in the concentration range from 1.0×10−9 to 1.0×10−7 mol L−1. The detection and quantification limits were found to be 3.0×10−10 mol L−1 and 1.0×10−9 mol L−1, respectively. The proposed method was successfully applied to ambazone determination in real samples.

Publisher

Journal

Year

Volume

12

Issue

12

Pages

1239-1245

Physical description

Dates

published
1 - 12 - 2014
online
7 - 6 - 2014

Contributors

  • University of Lodz
  • University of Lodz
  • University of Lodz
  • University of Lodz
  • University of Lodz

References

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-014-0574-7
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