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Number of results

Journal

2014 | 12 | 3 | 325-331

Article title

Determination of vitamin B6 (pyridoxine hydrochloride) based on a novel BZ oscillating reaction system catalyzed by a macrocyclic complex

Content

Title variants

Languages of publication

EN

Abstracts

EN
This paper reports a new method for determination of VB6 (pyridoxine hydrochloride) by its perturbation effects on a novel Belousov-Zhabotinskii (BZ) oscillating system. This novel BZ system, in which malic acid serves as the substrate, contains an enzyme-like complex, macrocyclic complex {[CuL](ClO4)2}, as catalyst. The ligand L in the complex is 5,7,7,12,14,14-hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene. Results show that the addition of pyridoxine hydrochloride can perturb the oscillation amplitude and period, and the change of the oscillation amplitude is linearly proportional to the concentration of pyridoxine hydrochloride in the range of 5×10−7−2.5×10−4 M. The obtained RSD with seven samples is 3.073%. An assay of pharmaceutical tablets of vitamin B6 was evaluated. Some foreign ions were studied with respect to their possible influence on the determination of pyridoxine hydrochloride. The factors which influence this reaction include the concentration of reactant, the temperature of the reaction, property of catalyst, etc. Furthermore, the possible reaction mechanism has been proposed using the Field-Körös-Noyes (FKN) model.

Publisher

Journal

Year

Volume

12

Issue

3

Pages

325-331

Physical description

Dates

published
1 - 3 - 2014
online
21 - 12 - 2013

Contributors

author
  • Anhui University
author
  • Anhui University
author
  • Anhui University
author
  • Anhui University
author
  • East China Jiaotong University

References

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-013-0383-4
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