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Number of results

Journal

2014 | 12 | 3 | 341-347

Article title

A low-cost automated flow analyzer based on low temperature co-fired ceramic and LED photometer for ascorbic acid determination

Content

Title variants

Languages of publication

EN

Abstracts

EN
An automated flow analyzer based on low temperature co-fired ceramic (LTCC), a solid-phase reactor (SPR) and a low-cost photometer was designed for ascorbic acid (AA) determination in pharmaceutical formulations. It consists of a peristaltic pump, three-way solenoid valves, SPR to chemically convert Cu(II) into Cu(I), and a LTCC device for mixing the liberated copper with bathocuproine and detection. The flow cell in the LTCC employed an ultrabright LED - photodiode photometer. The analyzer successfully determined AA in pharmaceutical formulations. The analytical curve from 8.5×10−6 to 7.0×10−4 M gave a detection limit of 7.0×10−7 M and a RSD of 2.1% for a 2.0×10−4 M AA solution (n = 10). A high sampling frequency of 102 h−1 and low reagent and sample consumption (150 µL) resulted.

Publisher

Journal

Year

Volume

12

Issue

3

Pages

341-347

Physical description

Dates

published
1 - 3 - 2014
online
21 - 12 - 2013

Contributors

  • Federal University of São Carlos
author
  • Federal University of São Carlos
  • Federal University of São Carlos
  • Federal University of Viçosa
  • Autonomous University of Barcelona
  • Federal University of São Carlos
author
  • Federal University of São Carlos

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-013-0377-2
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