Dispersive evaluation and surface chemistry of advanced, multifunctional silica/lignin hybrid biomaterials

• Authors: Magdalena Nowacka , Łukasz Klapiszewski , Małgorzata Norman , Teofil Jesionowski
• Languages of publication: EN

Abstracts

EN

Advanced silica/lignin hybrid biomaterials were obtained using hydrated or fumed silicas (Aerosil®200) and Kraft lignin as precursors, which is a cheap and biodegradable natural polymer. To extend the possible range of applications, the silicas were first modified with N-2-(aminoethyl)-3-aminopropyltrimethoxsysilane, and then with Kraft lignin, which had been oxidized with sodium periodate. The SiO2/lignin hybrids and precursors were characterised by means of determination of their physicochemical and dispersive-morphological properties. The effectiveness of silica binding to lignin was verified by FT-IR spectroscopy. The zeta potential value provides relevant information regarding interactions between colloid particles. Measurement of the zeta potential values enabled an indirect assessment of stability for the studied hybrid systems. Determination of zeta potential and density of surface charge also permitted the quantitative analysis of changes in surface charge, and indirectly confirmed the effectiveness of the proposed method for synthesis of SiO2/lignin hybrid materials. A particularly attractive feature for practical use is their stability, especially electrokinetic stability. It is expected that silica/lignin hybrids will find a wide range of applications (polymer fillers, biosorbents, electrochemical sensors), as they combine the unique properties of silica with the specific structural features of lignin. This makes these hybrids biomaterials advanced and multifunctional. [...]

Keywords

EN

Silica/lignin hybrid biomaterials; Surface functionalization; Physicochemical and structural properties; Zeta potential; Surface charge density

• Publisher: De Gruyter Open
• Journal: Open Chemistry
• Year: 2013
• Volume: 11
• Issue: 11
• Pages: 1860-1873

Dates

published

1 - 11 - 2013

online

25 - 8 - 2013

Contributors

author

Magdalena Nowacka

• Faculty of Chemical Technology, Institute of Chemical Technology and Engineering, Poznan University of Technology, PL-60965, Poznan, Poland

author

Łukasz Klapiszewski

• Faculty of Chemical Technology, Institute of Chemical Technology and Engineering, Poznan University of Technology, PL-60965, Poznan, Poland

author

Małgorzata Norman

• Faculty of Chemical Technology, Institute of Chemical Technology and Engineering, Poznan University of Technology, PL-60965, Poznan, Poland

author

Teofil Jesionowski

• Faculty of Chemical Technology, Institute of Chemical Technology and Engineering, Poznan University of Technology, PL-60965, Poznan, Poland

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Identifiers

DOI

10.2478/s11532-013-0322-4