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Number of results

Journal

2013 | 11 | 7 | 1150-1162

Article title

Five different columns in the analysis of basic drugs in hydrophilic interaction liquid chromatography

Content

Title variants

Languages of publication

EN

Abstracts

EN
Five different columns (two silica, two cyanopropyl and one diol) were investigated in hydrophilic interaction liquid chromatography (HILIC). For the assessment of columns behavior in HILIC mode, six basic drugs (lamotrigine, thioridazine, clozapine, chlorpheniramine, pheniramine and sulpiride) were chosen. The assessment of the influence of the concentration of organic modifier on analytes’ retention on each column was provided by fitting the retention data into theoretical models. Utilizing the statistical analysis, the selection of the model that provides better prediction of the retention behavior was enabled. Dual RP-HILIC mechanism was suggested on cyanopropyl and diol columns, therefore the transition points between the two mechanisms on these columns were calculated. Furthermore, in order to investigate the impact of three factors simultaneously on the retention behavior of the analyzed substances on Betasil Silica column, chemometrically-aided empirical models were built. The experiments were conducted according to the matrix of Box-Behnken design and on the basis of the retention data, six quadratic models were obtained and their adequacy was confirmed using ANOVA test. The obtained coefficients of quadratic models enabled the elucidation of both single factor and factor interactions influence. This was also graphically presented in 3D response surface plots. [...]

Publisher

Journal

Year

Volume

11

Issue

7

Pages

1150-1162

Physical description

Dates

published
1 - 7 - 2013
online
26 - 4 - 2013

Contributors

  • Department of Drug Analysis, University of Belgrade — Faculty of Pharmacy, 11221, Belgrade, Serbia
  • Department of Drug Analysis, University of Belgrade — Faculty of Pharmacy, 11221, Belgrade, Serbia
author
  • Department of Drug Analysis, University of Belgrade — Faculty of Pharmacy, 11221, Belgrade, Serbia
  • Department of Drug Analysis, University of Belgrade — Faculty of Pharmacy, 11221, Belgrade, Serbia
  • Department of Drug Analysis, University of Belgrade — Faculty of Pharmacy, 11221, Belgrade, Serbia
  • Department of Physical Chemistry and Instrumental Methods, University of Belgrade — Faculty of Pharmacy, 11221, Belgrade, Serbia

References

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-013-0245-0
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