Determination of lead in solution by solid phase extraction, elution, and spectrophotometric detection using 4-(2-pyridylazo)-resorcinol

• Authors: Ismail Rahman , Yoshiaki Furusho , Zinnat Begum , Rika Sato , Hiroshi Okumura , Hiroko Honda , Hiroshi Hasegawa
• Languages of publication: EN

Abstracts

EN

Lead (+2) was selectively adsorbed on a solid phase extraction (SPE) gel (molecular recognition technology, MRT), quantitatively extracted, and spectrophotometrically determined as the Pb(II)-PAR (4-(2-pyridylazo)-resorcinol) complex. The linear range was 0.01 to 0.75 mg L−1 and the detection limit was 6.4 µg L−1. The MRT-SPE allows selective Pb(II) extraction from complex ion-rich matrices, which is difficult with other techniques. Interference from common matrix ions such as Fe2+, Ni2+, Cu2+ or Co2+ is minimized. [...]

Keywords

EN

Lead; 4-(2-pyridylazo)-resorcinol; Colorimetric; Interferences; Solid phase extraction

• Publisher: De Gruyter Open
• Journal: Open Chemistry
• Year: 2013
• Volume: 11
• Issue: 5
• Pages: 672-678

Dates

published

1 - 5 - 2013

online

27 - 2 - 2013

Contributors

author

Ismail Rahman

author

Yoshiaki Furusho

• GL Sciences Inc., Nishishinjuku 6-22-1, Shinjuku, Tokyo, 163-1130, Japan

author

Zinnat Begum

• Graduate School of Natural Science and Technology, Kanazawa University, Kakuma, Kanazawa, 920-1192, Japan

author

Rika Sato

• Kyoritsu Chemical Check Lab., Corp., Ohta-ku, Tokyo, 145-0071, Japan

author

Hiroshi Okumura

• Kyoritsu Chemical Check Lab., Corp., Ohta-ku, Tokyo, 145-0071, Japan

author

Hiroko Honda

• Kyoritsu Chemical Check Lab., Corp., Ohta-ku, Tokyo, 145-0071, Japan

author

Hiroshi Hasegawa

• Institute of Science and Engineering, Kanazawa University, Kakuma, Kanazawa, 920-1192, Japan

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Identifiers

DOI

10.2478/s11532-013-0203-x