Considerations on the application of miniaturized sample preparation approaches for the analysis of organic compounds in environmental matrices

Pena-Pereira, Francisco; Duarte, Regina; Duarte, Armando

doi:10.2478/s11532-011-0114-7

Journal

Open Chemistry

2012 | 10 | 3 | 433-449

Article title

Considerations on the application of miniaturized sample preparation approaches for the analysis of organic compounds in environmental matrices

Authors

Francisco Pena-Pereira , Regina Duarte , Armando Duarte

Content

Full texts:

http://www.degruyter.com/view/j/chem.2012.10.issue-3/s11532-011-0114-7/s11532-011-0114-7.pdf [remote]

Title variants

Languages of publication

EN

Abstracts

EN

The miniaturization and improvement of sample preparation is a challenge that has been fulfilled up to a point in many fields of analytical chemistry. Particularly, the hyphenation of microextraction with advanced analytical techniques has allowed the monitoring of target analytes in a vast variety of environmental samples. Several benefits can be obtained when miniaturized techniques such as solid-phase microextraction (SPME) or liquid-phase microextraction (LPME) are applied, specifically, their easiness, rapidity and capability to separate and pre-concentrate target analytes with a negligible consumption of organic solvents. In spite of the great acceptance that these green sample preparation techniques have in environmental research, their full implementation has not been achieved or even attempted in some relevant environmental matrices. In this work, a critical review of the applications of LPME and SPME techniques to isolate and pre-concentrate traces of organic pollutants is provided. In addition, the influence of the environmental matrix on the effectiveness of LPME and SPME for isolating the target organic pollutants is addressed. Finally, unsolved issues that may hinder the application of these techniques for the extraction of dissolved organic matter from environmental samples and some suggestions for developing novel and less selective enrichment and isolation procedures for natural organic matter on the basis of SPME and LPME are included. [...]

Keywords

EN

Miniaturization Sample preparation Microextraction Environmental samples Natural organic matter

Publisher

De Gruyter Open

Journal

Open Chemistry

Year

2012

Volume

10

Issue

3

Pages

433-449

Physical description

Dates

published

1 - 6 - 2012

online

23 - 3 - 2012

Contributors

author

Francisco Pena-Pereira

CESAM & Department of Chemistry, University of Aveiro, 3810-193, Aveiro, Portugal

author

Regina Duarte

CESAM & Department of Chemistry, University of Aveiro, 3810-193, Aveiro, Portugal

author

Armando Duarte

aduarte@ua.pt

CESAM & Department of Chemistry, University of Aveiro, 3810-193, Aveiro, Portugal

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Document Type

Publication order reference

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DOI

10.2478/s11532-011-0114-7

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bwmeta1.element.-psjd-doi-10_2478_s11532-011-0114-7