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Number of results

Journal

2011 | 9 | 2 | 275-282

Article title

Synthesis and characterization of layered double hydroxides with different cations (Mg, Co, Ni, Al), decomposition and reformation of mixed metal oxides to layered structures

Content

Title variants

Languages of publication

EN

Abstracts

EN
Three layered double hydroxides (LDH) [Mg1−xAlx(OH)2]x+(Am−)x/m]·nH2O and [MII
1−xMIII
x (OH)2]x+(Am−)x/m]·nH2O (MII - Mg, Co, Ni; MIII - Al; A - CO3
2−) were successfully synthesized by the low supersaturation method. The as-synthesized LDH samples were thermally decomposed and the derived mixed metal oxides reformed back to layered structures in water and magnesium nitrate media at different temperatures. All synthesized samples were characterized by X-ray diffraction (XRD) analysis, thermogravimetric (TG) analysis, X-ray fluorescence (XRF) analysis and scanning electron microscopy (SEM). The results of XRD and XRF analyses showed that single-phase layered double hydroxides were formed during synthesis and reformation. It was demonstrated, that a partially substituted by cobalt and nickel LDH samples also show memory effect. The crystallite size of regenerated LDH depends on the regeneration media, temperature and chemical composition. The LDH samples after regeneration consist of large particles with sharp edges along with a large amount of smaller particles

Publisher

Journal

Year

Volume

9

Issue

2

Pages

275-282

Physical description

Dates

published
1 - 4 - 2011
online
17 - 2 - 2011

Contributors

  • Kaunas University of Technology
  • Nature Research Centre
  • Amiagus
  • Vilnius University

References

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-011-0007-9
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