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Number of results

Journal

2010 | 8 | 6 | 1323-1330

Article title

pH impact on the sol-gel preparation of calcium hydroxyapatite, Ca10(PO4)6(OH)2, using a novel complexing agent, DCTA

Content

Title variants

Languages of publication

EN

Abstracts

EN
Aqueous sol-gel chemistry routes - based on ammonium hydrogen phosphate as the phosphorus precursor, calcium acetate monohydrate as the source of calcium ions, and 1,2-diaminocyclohexanetetraacetic acid monohydrate (DCTA) as the complexing agent - have been used to prepare calcium hydroxyapatite (HA). The sol-gel process was performed in aqueous solution at different pH values followed by calcination of the dry precursor gels for 5 h at 1000°C. Phase transformations, composition, and structural changes in the polycrystalline samples were studied by thermoanalytical methods (TG/DTA), infrared spectroscopy (IR), X-ray powder diffraction analysis (XRD), and scanning electron microscopy (SEM). It was shown that pH adjustment has significant impact on the apatite formation process and on the morphology and phase purity of the ceramic samples.

Publisher

Journal

Year

Volume

8

Issue

6

Pages

1323-1330

Physical description

Dates

published
1 - 12 - 2010
online
8 - 10 - 2010

Contributors

  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania
  • Laboratory of Inorganic Materials, Tallinn University of Technology, 19086, Tallinn, Estonia
author
  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania
  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania
  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-010-0113-0
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