Full-text resources of PSJD and other databases are now available in the new Library of Science.
Visit https://bibliotekanauki.pl

PL EN


Preferences help
enabled [disable] Abstract
Number of results

Journal

2010 | 8 | 5 | 1059-1068

Article title

Preparation and characterization of high specific surface area Mn3O4 from electrolytic manganese residue

Content

Title variants

Languages of publication

EN

Abstracts

EN
Mn3O4 powders have been produced from Electrolytic Manganese Residue (EMR). After leaching of EMR in sulfuric acid, MnSO4 solution containing various ions was obtained. Purifying the solution obtained and then adding aqueous alkali to the purified MnSO4 solution, Mn(OH)2 was prepared. Two methods were employed to produce Mn3O4. One way was oxidation of Mn(OH)2 in aqueous phase under atmosphere pressure to obtain Mn3O4. The other way was roasting Mn(OH)2 precursors in the range of 500°C to 700°C. The prepared samples were investigated by using several techniques including X-ray powder diffraction (XRD), Fourier Transformation Infra-Red (FTIR) spectra, and Brunauer-Emmett-Teller (BET) specific surface area instrument. Particle distribution and magnetic measurements were carried out on laser particle size analyzer, vibrating sample magnetometer (VSM). Through XRD, FTIR and determination of total Mn content (TMC), the products prepared were confirmed to be a single phase Mn3O4. BET specific surface areas can reach to 32 m2 g−1. The results indicated that products synthesized by aqueous solution oxidation method had higher specific surface areas and smaller particle size than those prepared by means of roasting. However the products prepared using the above two methods showed no obvious differences in magnetic property. [...]

Keywords

Publisher

Journal

Year

Volume

8

Issue

5

Pages

1059-1068

Physical description

Dates

published
1 - 10 - 2010
online
5 - 9 - 2010

Contributors

author
  • Department of Resources and Environmental Science, Key Laboratory for the Exploitation of Southwest Resources and Environmental Disaster Control Engineering of Ministry of Education, Chongqing University, 400044, Chongqing, P.R. China
author
  • Department of Resources and Environmental Science, Key Laboratory for the Exploitation of Southwest Resources and Environmental Disaster Control Engineering of Ministry of Education, Chongqing University, 400044, Chongqing, P.R. China
  • Department of Resources and Environmental Science, Key Laboratory for the Exploitation of Southwest Resources and Environmental Disaster Control Engineering of Ministry of Education, Chongqing University, 400044, Chongqing, P.R. China

References

  • [1] M. Baldi, F. Milella, G. Ramis, V. Sanchez Escribano, G. Busca, Appl. Catal. A Gen. 166, 75 (1998) http://dx.doi.org/10.1016/S0926-860X(97)00242-1[Crossref]
  • [2] A.V. Olmos, R. Redon, G.R. Gattorno, M.E.M. Zamora, F.M. Leal, A.L.F. Osorio, J.M. Saniger, J. Colloid Sci. 291, 175 (2005) http://dx.doi.org/10.1016/j.jcis.2005.05.005[Crossref]
  • [3] W.M. Wang, Y.N. Yang, J.Y. Zhang, Appl. Catal. A 133, 81 (1995) http://dx.doi.org/10.1016/0926-860X(95)00186-7[Crossref]
  • [4] M. Baldi, E. Finonnhio, F. Milella, G. Busca, Appl. Catal. B: Environ. 16, 43 (1998) http://dx.doi.org/10.1016/S0926-3373(97)00061-1[Crossref]
  • [5] M.C. Bernard, H.L. Goff, B.V. Thi, J. Electrochem. Soc. 140, 3065 (1993) http://dx.doi.org/10.1149/1.2220986[Crossref]
  • [6] Y. Yamashita, K. Mukai, J. Yoshinobu, M. Lippmaa, T. Kinoshita, M. Kawasaki, Surf. Sci. 514, 54 (2002) http://dx.doi.org/10.1016/S0039-6028(02)01607-2[Crossref]
  • [7] V. Berbenni, A. Marini, J. Anal. Appl. Pyrolysis 70, 437 (2003) http://dx.doi.org/10.1016/S0165-2370(03)00003-2[Crossref]
  • [8] L. Sanchez, J. Farcy, J. Tirado, J. Mater. Chem. 6, 37 (1996) http://dx.doi.org/10.1039/jm9960600037[Crossref]
  • [9] W. Wang, C. Xu, G. Wang, Y. Liu, C. Zheng, Adv. Mater. 14, 837 (2002) http://dx.doi.org/10.1002/1521-4095(20020605)14:11<837::AID-ADMA837>3.0.CO;2-4[Crossref]
  • [10] W. Zhang, Z. Yang, Y. Liu, S. Tang, X. Han, M. Chen, J. Cryst. Growth 263, 394 (2004) http://dx.doi.org/10.1016/j.jcrysgro.2003.11.099[Crossref]
  • [11] Z. Weixin, W. Cheng, Z. Xiaoming, X. Yi, Q. Yitai, Solid State Ion. 117, 331 (1999) http://dx.doi.org/10.1016/S0167-2738(98)00432-9[Crossref]
  • [12] J.C. Southard, G.E. Moore, J. Am. Chem. Soc. 64, 1769 (1942) http://dx.doi.org/10.1021/ja01260a007[Crossref]
  • [13] E. Finocchio, G. Busca, Catal. Today 70, 213 (2001) http://dx.doi.org/10.1016/S0920-5861(01)00419-9[Crossref]
  • [14] Y.C. Zhang, T. Qiao, X.Y. Hu, J. Solid State Chem. 177, 4093 (2004) http://dx.doi.org/10.1016/j.jssc.2004.05.034[Crossref]
  • [15] G. Demazeau, J. Mater. Chem. 9, 15 (1999) http://dx.doi.org/10.1039/a805536j[Crossref]
  • [16] Y.Q. Chang, X.Y. Xu, X.H. Luo, C.P. Chen, D.P. Yu, J. Cryst. Growth 264, 32 (2004) http://dx.doi.org/10.1016/j.jcrysgro.2003.11.117[Crossref]
  • [17] S.K. Apte, S.D. Naik, R.S. Sonawane, B.B. Kale, N. Pavaskar, A.B. Mandale, B.K. Das, Mater. Res. Bull. 41, 647 (2006) http://dx.doi.org/10.1016/j.materresbull.2005.08.028[Crossref]
  • [18] M. Anilkumar, V. Ravi, Mater. Res. Bull. 40, 605 (2005) http://dx.doi.org/10.1016/j.materresbull.2005.01.009[Crossref]
  • [19] A. Baykal, Y. Köseoǧlu, M. Senel, Central Eur. J. Chem. 5, 169 (2007) http://dx.doi.org/10.2478/s11532-006-0064-7[Crossref]
  • [20] O.Yu. Gorbenko, I.E. Graboy, V.A. Amelichev, A.A. Bosak, A.R. Kaul, B. Guttler, V.L. Svetchnikov, H.W. Zandbergen, Solid State Commun. 124, 15 (2002) http://dx.doi.org/10.1016/S0038-1098(02)00470-2[Crossref]
  • [21] A. Askarinejad, A. Morsali, Ultrason Sonochem 16, 124 (2009) http://dx.doi.org/10.1016/j.ultsonch.2008.05.015[Crossref]
  • [22] Z.W. Chen, J.K.L. Lai, C.H. Shek, Scr. Mater. 55, 735 (2006) http://dx.doi.org/10.1016/j.scriptamat.2006.05.041[Crossref]
  • [23] T. Ozkaya, A. Baykal, H. Kavas, Physica B-Condensed Matter. 403, 19 (2008) http://dx.doi.org/10.1016/j.physb.2008.07.002[Crossref]
  • [24] Z. Weixin, W. Cheng, Z. Xiaoming, X. Yi, Q. Yitai, Solid State Ionics 117, 331 (1999) http://dx.doi.org/10.1016/S0167-2738(98)00432-9[Crossref]
  • [25] J.M. Boyero, E.L. Fernández, J.M. Gallardo-Amores, R.C. Ruano, V.E. Sánchez, E.B. Pérez, Int. J. Inorg. Mater. 3, 889 (2001) http://dx.doi.org/10.1016/S1466-6049(01)00091-5[Crossref]
  • [26] F.A. Al Sagheer, M.A. Hasan, L. Pasupulety, M.I. Kaki, J. Mater. Sci. Lett. 18, 209 (1999) http://dx.doi.org/10.1023/A:1006620114539[Crossref]
  • [27] B. Gillot, M. El. Guendouzi, M. Laarj, Materials Chemistry and Physics 70, 1 (2001) http://dx.doi.org/10.1016/S0254-0584(00)00473-9[Crossref]
  • [28] S. Brunauer, L. Deming, W. Deming, E. Teller, J. Am. Chem. Soc. 62, 7 (1940) http://dx.doi.org/10.1021/ja01858a003[Crossref]
  • [29] K.S.W. Sing, D.H. Everett, R.A.W. Haul, Pure & Appl. Chem. 57, 4 (1985) http://dx.doi.org/10.1351/pac198557040603[Crossref]
  • [30] J. Rouquerol, D. Avnir, C.W. Fairbridge, Pure & Appl. Chem. 66, 8 (1994) http://dx.doi.org/10.1351/pac199466081739[Crossref]

Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-010-0081-4
JavaScript is turned off in your web browser. Turn it on to take full advantage of this site, then refresh the page.