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Number of results

Journal

2009 | 7 | 1 | 66-73

Article title

Synthesis and structural characterization of amino-functionalized polysaccharides

Content

Title variants

Languages of publication

EN

Abstracts

EN
A variety of carbohydrates, in particular polysaccharides can be subjected to chemical modification to obtain derivatives with amphiphilic properties, which enable biochemical or biological reactions at the polymer surface. In the present work, a polydisperse maltodextrin mixture of average molecular weight 3000 was coupled with 1,6-hexamethylenediamine (HMD) via reductive amination reaction. Resulting products were characterized by thermal analysis and positive nanoelectrospray quadrupole time-of-flight (Q-TOF) mass spectrometry (MS) and tandem mass spectrometry (MS/MS). Both thermal analysis and MS screening confirmed the formation of the HMD-polysaccharide coupling products. Moreover, HMD-linked polysaccharide chains containing 2 to 26 glucose building blocks were identified by nanoESI Q-TOF MS. MS/MS fragmentation using collision-induced dissociation (CID) at low ion acceleration energies provided strong evidence for HMD-maltodextrin linkage formation and the set of sequence ions diagnostic for the composition and structure of a HMD-linked chain containing 18 glucose residues. [...]

Publisher

Journal

Year

Volume

7

Issue

1

Pages

66-73

Physical description

Dates

published
1 - 3 - 2009
online
23 - 12 - 2008

Contributors

author
  • Institute of Chemistry, Romanian Academy, RO-300223, Timisoara, Romania
author
  • Department of Chemical and Biological Sciences, “Aurel Vlaicu” University of Arad, Romania, RO-310130, Arad, Romania
author
  • Department of Chemical and Biological Sciences, “Aurel Vlaicu” University of Arad, Romania, RO-310130, Arad, Romania
author
  • Faculty of Industrial Chemistry and Environment Engineering, “Politehnica” University of Timisoara, RO-300030, Timisoara, Romania
author
author

References

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-008-0090-8
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