Estimation of platinum in environmental water samples with solid phase extraction technique using inductively coupled plasma mass spectrometry

• Authors: Aleksandra Dubiella-Jackowska , Żaneta Polkowska , Lech Dariusz , Piotr Pasławski , Wojciech Staszek , Jacek Namieśnik
• Languages of publication: EN

Abstracts

EN

A solid phase extraction technique for the determination of platinum(IV) at trace levels by inductively coupled plasma mass spectromA solid phase extraction technique for the determination of platinum(IV) at trace levels by inductively coupled plasma mass spectrometry (ICP-MS) was developed. The method was based on retention of platinum in a sample on silica gel modified with aminepropyl groups. The retention of platinum(IV) from the sample solution and the recovery of platinum with 1.0 mol L−1 thiourea solution were quantitative. The relative standard deviation (RSD) was calculated as 5% (n = 7) at the 10 ng L−1 level. The enrichment factor was found to be (50-fold) for 250 mL of water sample. Under optimum conditions, the method detection limit (MDL) was found to be 1 ng L−1 for platinum in water matrices. Recoveries of Pt from spike addition to atmospheric water samples were quantitative (80–95%). The present method was used for the determination of platinum in precipitation, throughfall and runoff water samples. [...]

Keywords

EN

Platinum; SPE; Inductively coupled plasma mass spectrometry (ICP-MS); Atmospheric waters

• Publisher: De Gruyter Open
• Journal: Open Chemistry
• Year: 2009
• Volume: 7
• Issue: 1
• Pages: 35-41

Dates

published

1 - 3 - 2009

online

23 - 12 - 2008

Contributors

author

Aleksandra Dubiella-Jackowska

• Department of Analytical Chemistry, Chemical Faculty, Gdansk University of Technology, 80-952, Gdansk, Poland

author

Żaneta Polkowska

• Department of Analytical Chemistry, Chemical Faculty, Gdansk University of Technology, 80-952, Gdansk, Poland

author

Lech Dariusz

• Central Chemical Laboratory, Polish Geological Institute, 00-975, Warsaw, Poland

author

Piotr Pasławski

• Central Chemical Laboratory, Polish Geological Institute, 00-975, Warsaw, Poland

author

Wojciech Staszek

• Faculty of Physical Geography and Environmental Protection, University of Gdańsk, 80-246, Gdańsk, Poland

author

Jacek Namieśnik

• Department of Analytical Chemistry, Chemical Faculty, Gdansk University of Technology, 80-952, Gdansk, Poland

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Identifiers

DOI

10.2478/s11532-008-0081-9