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Number of results

Journal

2008 | 6 | 2 | 216-221

Article title

Influence of EDTA, carboxylic acids, amino- and hydroxocarboxylic acids and monosaccharides on the generation of arsines in hydride generation atomic absorption spectrometry

Content

Title variants

Languages of publication

EN

Abstracts

EN
The influence of EDTA, carboxylic acids, amino-and hydroxocarboxylic acids, monosaccharides and humic substances on the generation of arsines in hydride generation atomic absorption spectrometry (HGAAS) was investigated. EDTA (0.02 mol L−1), ascorbic acid (0.02 mol L−1) and glucose or fructose (0.2 mol L−1) are useful additives for levelling sensitivities for As(III), monomethylarsonate (MMA) and dimethylarsinate (DMA). The presence of glycine, malonic, tartaric acids, BICIN and soil humin extracts leads to differences in analytical signal response between these arsenic species. An analytical application to the determination of the sum of As(III), monomethylarsonate (MMA) and dimethylarsinate (DMA) as well as the sum of toxicologically relevant hydride forming arsenic fraction As(III) + As(V) + MMA + DMA in EDTA soil/sediment extracts using continuous flow HGAAS was demonstrated. The limit of detection was 0.2 mg kg−1 As. Within-day and between-day precision were in the range 3–7% and 4–10%, respectively, for arsenic contents of 0.7–25 mg kg−1, with recoveries 95–103%. [...]

Publisher

Journal

Year

Volume

6

Issue

2

Pages

216-221

Physical description

Dates

published
1 - 6 - 2008
online
17 - 4 - 2008

Contributors

  • Faculty of Chemistry, University of Sofia, 1 James Bourchier Blvd., Sofia, 1164, Bulgaria
  • Institute of Chemistry, Faculty of Science, Sts. Cyril and Methodius University, POB 162, MK-1000, Skopje, Republic of Macedonia
  • Faculty of Chemistry, University of Sofia, 1 James Bourchier Blvd., Sofia, 1164, Bulgaria
  • Faculty of Chemistry, University of Sofia, 1 James Bourchier Blvd., Sofia, 1164, Bulgaria
  • Institute of Chemistry, Faculty of Science, Sts. Cyril and Methodius University, POB 162, MK-1000, Skopje, Republic of Macedonia

References

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-008-0006-7
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