Design of experiment in the development of
spme method for the determination of pesticide
residues in fruits and vegetables

• Authors: Lukman Bola Abdulra’uf , Guan Huat Tan
• Languages of publication: EN

Abstracts

EN

The various microextraction techniques have
been developed in order to reduce sample preparation
time, improve sensitivity and selectivity as well as to
corroborate the recent advances in the development of
highly sensitive and efficient analytical instrumentation.
The current trend is aimed at the simplification and
miniaturization of extraction steps, which has led to
the combination of multi-step extraction and analytical
analysis into single uninterrupted step. The method
development involves the screening and subsequent
optimization of both gas chromatography-mass
spectrometry (GC-MS) and solid phase microextraction
(SPME) parameters using multivariate experimental
design, which has been shown to be efficient and effective
with little experimental runs. The use of microextraction
has been very effective in the analysis of contaminants in
food, water and the environments to ensure they are safe
and does not pose any health risk to human.

Keywords

EN

GC-MS; SPME; multivariate experimentaldesign; contaminants

• Publisher: De Gruyter Open
• Journal: Sample Preparation
• Year: 2014
• Volume: 2
• Issue: 1

Dates

received

1 - 12 - 2014

accepted

1 - 5 - 2015

online

8 - 7 - 2015

Contributors

author

Lukman Bola Abdulra’uf

• Department of
  Chemical, Geological and Physical Sciences, College of Pure and
  Applied Sciences, Kwara State University, Malete, P.M.B. 1530, Ilorin,
  Kwara State
• Department of Chemistry,
  Faculty of Science, University of Malaya, 50603, Pantai Valley, Kuala
  Lumpur, Malaysia

author

Guan Huat Tan

• Department of Chemistry,
  Faculty of Science, University of Malaya, 50603, Pantai Valley, Kuala
  Lumpur, Malaysia

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Identifiers

DOI

10.1515/sampre-2015-0005