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EN
The aim of this study is the evaluation of the effect of chemical treatment of jute fibres on their permeability with polyester resin and determination of optimal treatment parameters. Unmodified jute fabric by LENTEX, Poland and polyester resin ESTROMAL 14 were used in the experiments. NaOH and KOH water solutions (various concentration - from 1 to 15% - and treatment duration - from 0.5 to 6h), vinyl acetate, methanol, toluene diizocyanate were used for the treatment. Determination of the effect of the chemical treatment on fiber-resin interaction was made in: infiltration of resin into reinforcement structure tests and fabric absorbability tests. Three criteria: time of penetration of resin into the reinforcing fabric, fabric absorbability and the area of a part of the specimen cross-section penetrated with the resin were taken into account. The fabrics treated with 1-5% - long-time and 15% short-time NaOH and KOH water solutions showed the best results within the tested criteria. These results do not correspondent directly with the mechanical properties of cured composites manufactured on the base of the treated fabrics. Alkali- and organic treatments significantly improve the mechanical performance of natural fibres reinforced composites, but organic treatments (methanol, toluene diisocyanate) gives better improvement in mechanical properties in comparison with the alkali-treatments. The measurement methods applied in the study may be generally useful in the evaluation of the effect of chemical treatment of natural fibres on their wettability with the liquid matrix.
EN
The paper presents determination of the effect of various chemical treatment on the strength of 288 tex jute yarn arisen from the plain weave fabric produced by LENTEX, Poland. The yarn was put to alternative treatments in: NaOH and KOH water solutions with various concentration (from 1 to 15%) and treatment duration (from 0.5 to 6 hours), vinyl acetate, methanol and toluene diisocyanate. After the treatment it was put to tensile tests. Yarn diameter and elementary fibre twist angle were also measured using MICRO PROF FRT optical profilographometer. The SEM micro-photographs have also been performed in order to evaluate the structural changes of the yarn after the treatment.Optimal conditions of alcali-treatment are: 5% concentration and 2h duration for NaOH, 3% concentration and 4h duration for KOH. Such treatments give a growth in yarn rupture force up to 10% and they are well applicable in composite materials manufacturing. Also interaction with vinyl acetate and toluene diisocyanate has practically not negative influence on the mechanical performance of the yarn. Two effects were observed which can explain the influence of chemical treatment on mechanical performance of jute yarn: swelling and change in the orientation of elementary fibres.
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