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1

Efficiency of Linear and Non-Linear Classifiers for Gas Identification from Electrocatalytic Gas Sensor

100%

Kalinowski P., Woźniak Ł., Strzelczyk A., Jasinski P., Jasiński G.

Metrology and Measurement Systems

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2013

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issue 3

2

Point-of-Care Testing – Biosensor for Norepinephrine Determination

100%

Baluta S., Swist A., Cabaj J., Malecha K., Baluta S., Swist A., Cabaj J., Malecha K.

International Journal of Electronics and Telecommunications

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2020

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vol. 66

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issue 2

3

Voltammetric quantitation at the mercury electrode of the anticholinergic drug flavoxate hydrochloride in bulk and in a pharmaceutical formulation

100%

Ghoneim M. M., El-Attar M. A., Razeq S. A.

Open Chemistry

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2007

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vol. 5

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issue 2

496-507

EN

Flavoxate hydrochloride, 2-piperidinoethyl 3-methyl-4-oxo-2-phenyl-4-H-chromene-8-carboxylate, is a smooth muscle antispasmodic. Its electrochemical behavior was studied at the mercury electrode in buffered solutions containing 30% (v/v) methanol using dc-polarography, differential-pulse polarography, cyclic voltammetry, and linear sweep-and square-wave adsorptive stripping voltammetry. Sensitive and precise procedures were developed for determination of bulk flavoxate hydrochloride and in the pharmaceutical formulation Genurin® S.F, without sample pretreatment or extraction. Limits of quantitation (LOQ) of 1 × 10−5, 5 × 10−6, 1 × 10−8 and 1 × 10−9 M flavoxate hydrochloride were achieved by dc-polarography, differential-pulse polarography, linear sweep and square-wave adsorptive stripping voltammetric, respectively. [...]

4

New homodi-and heterotrinuclear metal complexes of Schiff base compartmental ligand: interaction studies of copper complexes with calf thymus DNA

100%

Mathur S., Tabassum S.

Open Chemistry

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2006

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vol. 4

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issue 3

502-522

EN

The new homodinuclear complexes 1–4 of the type [LMII 2Cl2], heterotrinuclear complexes 5 and 6 of the type [LMII 2SnIVCl6] where M = CuII, MnII, CoII, NiII and CuII and NiII, respectively have been synthesized and characterized by elemental analysis and various spectroscopic techniques. The homodinuclear complexes possess two different environments (N2 and N2O2donor sets) for holding the metal ions. The metal ion in N2 set exhibits square planar geometry with two chloride ions in the inner sphere but rhombic structure is found in tetradentate N2O2 Schiff base cavity while in heterotrinuclear complexes SnIV atom is in the octahedral environment. The interaction of complexes 1 and 5 with calf thymus DNA was carried out by absorption spectroscopy and cyclic voltammetry. The intrinsic binding constants (K b) of complex 1 and 5 were determined as 3.2 × 103 M−1 and 9.6 × 103 M−1, respectively suggesting that complex 5 binds more strongly to CT-DNA than complex 1. Fluorescence studies along with viscosity measurements have also been checked to authenticate the binding of metal complexes with DNA.

5

Voltammetric and potentiometric studies of some sulpha drug-Schiff base compounds and their metal complexes

100%

Ghoneim M., Mabrouk E., Hassanein A., El-Attar M., Hesham E.

Open Chemistry

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2007

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vol. 5

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issue 3

898-911

EN

The electrochemical behavior of some sulpha drug-Schiff bases at a mercury electrode was examined in the Britton-Robinson universal buffer of various pH values (2.5–11.7) containing 20% v/v) of ethanol using DC-polarography, cyclic voltammetry and controlled-potential electrolysis. The DC-polarograms and cyclic voltammograms of the examined compounds exhibited a single, 2-electron, irreversible, diffusion-controlled cathodic step within the entire pH range which is attributed to the reduction of the azomethine group-CH=N- to -CH2-NH-. The symmetry transfer coefficient (α) of the electrode reaction and the diffusion coefficient (D 0) of the reactant species were determined. The electrode reaction pathway of the compounds at the mercury electrode was suggested to follow the sequence: H+, e−, e−, H+. The dissociation constant of the sulpha drug-Schiff bases, the stability constant and stoichiometry of their complexes with various divalent transition metal ions (Mn2+, Co2+, Ni2+, Cu2+ and Zn2+) were determined potentiometrically at room temperature. [...]

6

Electrorefining of Indium Metal From Impure In-Sn Alloy in Fluoride Molten Salt

100%

Lee H.-G., Choi S.-H., Sim J.-J., Lim J.-H., Hyun S.-K., Lee J.-H., Park K.-T.

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2019

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vol. 64

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issue 3

7

Electrochemical sensors based on TiO2–Fe2O3 coupled system

100%

Kusior A., Karoń I., Radecka M., Kusior A., Karoń I., Radecka M.

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Refine search results

Efficiency of Linear and Non-Linear Classifiers for Gas Identification from Electrocatalytic Gas Sensor

Point-of-Care Testing – Biosensor for Norepinephrine Determination

Voltammetric quantitation at the mercury electrode of the anticholinergic drug flavoxate hydrochloride in bulk and in a pharmaceutical formulation

New homodi-and heterotrinuclear metal complexes of Schiff base compartmental ligand: interaction studies of copper complexes with calf thymus DNA

Voltammetric and potentiometric studies of some sulpha drug-Schiff base compounds and their metal complexes

Electrorefining of Indium Metal From Impure In-Sn Alloy in Fluoride Molten Salt

Electrochemical sensors based on TiO2–Fe2O3 coupled system