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BIOPOLYMER COMPOSITES BASED ON LIGNIN AND MICROCRYSTALLINE CHITOSAN

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Kopania E., Wiśniewska-Wrona M.
Progress on Chemistry and Application of Chitin and its Derivatives
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2016
|
vol. 21
122-134
EN
The article presents method of extracting lignin from hardwood and softwood after chemical treatment. Lignin fractions were extracted from black liquid (the by-product of pulp and paper industry), in a different reaction environment. Biopolymer composites were obtained by combining extracted lignin fraction and microcrystalline chitosan, which can be used as preparations for innovative biopolymer materials that are applicable in medical and hygienic products. The studies were performed in order to evaluate MCCh/Lignin composites to suitability to construction of dressing materials in the form of sponges. The MCCh/Lignin composites were tested for different properties: mechanical, sorption and absorption. The obtained lignin fractions and MCCh/Lignin composites were characterized by different structures and chemical purity as confirmed by FTIR spectra.
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BIOPOLYMER COMPOSITES BASED ON GALACTOGLUCOMANNANS (GGMS) AND MICRYSTALINE CHITOSAN (MCCH)

86%
Kopania E., Wiśniewska-Wrona M.
Progress on Chemistry and Application of Chitin and its Derivatives
|
2015
|
vol. 20
110-121
EN
The article presents a method of extracting galactoglucomannas (GGMs) from softwood (spruce). GGMs were extracted using thermal and enzymatic treatment in an aqueous environment. The extracted GGMs, depending on the extraction method, were characterized by different composition of simple carbohydrates i.e. glucose, galactose and mannose, as well as by the average molecular weight. Evaluation of the composition of GGMs obtained was performed using GC/MS and SEC. Biopolymer composites were obtained by combining GGMs and microcrystalline chitosan (MCCh), which can be used as preparations for plant protection and growth stimulation. The studies were performed in order to evaluate biological activity of composites based on Petri dish test in which their ability to stimulate seed germination of selected plants was estimated. The effect of plant growth stimulation depended on GGMs composition of simple carbohydrates. GC/MS and SEC chromatographic tests and 13C NMR analysis enabled to establish the composition and structural changes of the obtained GGMs and biocomposites
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