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One step synthesis of Diflunisal using a Pd-diamine complex

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Kylmälä T., Tois J., Xu Y., Franzén R.
Open Chemistry
|
2009
|
vol. 7
|
issue 4
818-826
EN
Diflunisal and Felbinac, two FDA-approved NSAIDs and other biphenyl carboxylic acids were prepared in one step by a simple and clean Suzuki cross-coupling reaction using an easily synthesized, air and moisture stable, palladium-diamine complex. The yield (93%) for the one-step preparation of Diflunisal is the best reported without using a glovebox and a phoshine-based catalyst. [...]
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