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Synthesis and crystal structure of 1-ethyl-3-(phenyl)-1,2,3-triazolium percholorate

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Doreswamy B., Mahendra M., Anandalwar S., Prasad J., Mantelingu K., Basappa, Rangappa K.

Open Chemistry

2003

vol. 1

issue 4

477-490

The isolation of stable carbenes of the Arduengo (1a) and Wanzlick (2a) type has prompted us to look for stable nitrenium ions of the related structural type 1-ethyl-3-(phenyl)-1,2,3-triazolium perchlorate (6+). The title compound C10H14Cl N3O4 was isolated and structure was investigated by X-ray crystallography. It crystallizes in the monoclinic space group P21/c with cell parameters a=6.697(4) Å, b=9.724(9) Å, c=19.844(2) Å and Z=4. The final residual factor is R1=0.0471 for 1545 reflections with I>2σ(I). The structure exhibits intermolecular hydrogen bonds.

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1 Open Chemistry

1 2003

1 Anandalwar S.

1 Basappa

1 Doreswamy B.

1 Mahendra M.

1 Mantelingu K.

1 Prasad J.

1 Rangappa K.

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Synthesis and crystal structure of 1-ethyl-3-(phenyl)-1,2,3-triazolium percholorate