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1H NMR and spectrophotometric study of alkaline metal ion complexes with N-dansyl aza-18-crown-6

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Ossowski T., Sulowska1 H., Karbowiak T., Zarzeczanska D., Gierczyk B., Schroeder G.
Open Chemistry
|
2006
|
vol. 4
|
issue 1
13-28
EN
Formation of complexes of A18C6-Dns and metal cations (Ca2+, Sr2+, Ba2+ and Mg2+) in acetonitrile has been studied by NMR, absorption and fluorescence spectroscopy and PM5 semi-empirical methods. A18C6-Dns forms stable complexes with Ca2+, Sr2+ and Ba2+ cations. The stability constants of various complexes are determined by different methods and their structures are visualised by the PM5 semi-empirical calculations.
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