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  1. 1 Open Chemistry

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  1. 1 2010

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  1. 1 Narayana B.

  2. 1 Sreevidya T.

  3. 1 Yathirajan H.

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Synthesis and characterization of some chalcones and their cyclohexenone derivatives

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Sreevidya T., Narayana B., Yathirajan H.
Open Chemistry
|
2010
|
vol. 8
|
issue 1
174-181
EN
A series of chalcones and their derivatives have been synthesized. Chalcones, 1-(1,3-benzodioxol-5-yl)-3-(aryl)-prop-2-en-1-ones were prepared by the aldol condensation of 1-(1,3-benzodioxol-5-yl)ethanones and aryl aldehydes. Based-catalyzed condensation of 1-(1,3-benzodioxol-5-yl)-3-(aryl)prop-2-en-1-ones with ethyl acetoacetate yields corresponding ethyl 4-(1,3-benzodioxol-5-yl)-6-(aryl)-2-oxocyclohex-3-ene-1-carboxylates. Some of the synthesized chalcones were reported in the literature; the newly synthesized compounds were characterized by single crystal X-ray studies, IR, 1H-NMR and LCMS mass spectral analysis. [...]
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