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  1. 1 Open Chemistry

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  1. 1 2013

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  1. 1 Beldean-Galea M.

  2. 1 Thiebaut D.

  3. 1 Vial J.

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Development of a screening method for the determination of xenobiotic organic pollutants in municipal landfill leachate using solvent extraction and comprehensive GCxGC-qMS analysis

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Beldean-Galea M., Vial J., Thiebaut D.
Open Chemistry
|
2013
|
vol. 11
|
issue 10
1563-1574
EN
In the present study, we propose a method for the evaluation of different classes of xenobiotic organic compounds enclosed in the municipal landfill leachate using comprehensive two-dimensional gas chromatography coupled with quadrupole mass spectrometry (GCxGC-qMS). Here we show that, due to high peak capacity of comprehensive two-dimensional gas chromatography, in a single run it is possible to separate compounds with different physical-chemical properties (such as aliphatic and aromatic compounds, polyaromatic hydrocarbons, phenols, phthalates, aldehydes, ketones, nitrogen containing compounds, organo-phosphoric flame retardants etc.), compounds which have proved to be endocrine disruptors, compounds that are persistent, bioaccumulative and toxic, carcinogenic, mutagenic, teratogenic, reprotoxic or harmful for the environment. Even though a solvent extraction method has been optimised, the extraction step still remains the main problem for a comprehensive characterization of all classes of organic toxicants enclosed in the municipal landfill leachate. [...]
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