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Coulometric determination of dithiphosphates with the use of the induced iodine-azide reaction

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Ciesielski W., Jędrzejewski W., Department of Instrumental Analysis U. o. Ł.
Acta Universitatis Lodziensis. Folia Chimica
|
1993
|
vol. 10
EN
The characteristics of potassium diethyl- and dibuthyldithiophosphates as the inductors of iodine-azide reaction carried out electrolytically have been presented. The influence of the pH and concentrations of azide and iodide ions on the course of reaction was examined. The determinations have been carried out in the range of 1-20 nmol.
PL
Przedstawiono charakterystykę dietylo- i dibutyloditiofosforanów jako induktorów reakcji jodo-azydkowej. Zbadano wpływ pH oraz stężeń azydku i jodku na przebieg reakcji. Oznaczenia kulometryczne przeprowadzono w zakresie 1-20 nmoli w próbce.
2
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Coulometric Determination of Sulphur Compounds Using the Induced lodine-Azide Reaction

100%
Ciesielski W., Department of Instrumental Analysis U. o. Ł.
Acta Universitatis Lodziensis. Folia Chimica
|
2004
|
vol. 13
PL
Wydrukowano z dostarczonych Wydawnictwu UŁ gotowych materiałów
EN
The review summarizes application of coulometry for determination of the sulphur compounds that induce the iodine-azide reaction. The article discusses advantages of the coulometric method. The influence of potassium iodide on induction coefficients is also described. Moreover, determination ranges of several inductors are presented and sensitivities of determination by different methods are compared.
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