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^{13}C High Resolution NMR Study of Methyl-Diethyl Sulfonium TCNQ 1:2 Complex

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Firlej L., Pęcherz J., Bernier P.
Acta Physica Polonica A
|
1995
|
vol. 87
|
issue 4-5
829-834
EN
Solid state high resolution ^{13}C NMR studies of a 1 : 2 charge transfer complex of TCNQ with diethyl-methyl sulfonium S + Et_{2}Me(TCNQ)_{2} are presented. The metallic shifts of TCNQ resonances are interpreted as due to the Pauli paramagnetism of conducting electrons and quantitatively con­nected with inhomogeneous spin density distribution over (TCNQ2)¯ dimer. A singularity of NMR parameters at T = 330 K is observed and described as a structural phase transition occurring in the S + Et_{2}Me cation sublattice.
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