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The FeBe_{2,5,11} compounds and theα-Fe(Be) solid solution of Be_xFe_{1-x} system were synthesized by laser irradiation from a powder mixture. The dependence of the phase structure on the initial sample composition (x=0.1-0.95) was studied. The phases were determined and studied by means of Mössbauer spectroscopy and X-ray diffraction.
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