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Mechanochemical Synthesis of Silver Chloride Nanoparticles by a Dilution Method in the System NH_4Cl-AgNO_3-NH_4NO_3

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Tatykaev B., Burkitbayev M., Uralbekov B., Urakaev F.
Acta Physica Polonica A
|
2014
|
vol. 126
|
issue 4
1044-1048
EN
This study presents the results of the synthesis of silver chloride nanoparticles dispersed within ammonium nitrate matrix via displacement mechanochemical reaction NH_{4}Cl + AgNO_{3} + zNH_{4}NO_{3} = (z+1)NH_{4}NO_{3} + AgCl at z = z_{1}= 7.22 and z = z_{2}= 3.64. The intermediate compound, NH_{4}Ag(NO_{3})_{2}, was identified after mechanochemical processing of studied system. Use of simultaneous thermogravimetry and differential scanning calorimetry provide a new means for preparing silver chloride nanoparticles in their free form by thermal treatment.
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