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Microwave Sintered Fe/MgO Soft Magnetic Composite

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EN
Micro/nano soft magnetic composite based on the Fe microparticles and the MgO nanoparticles was prepared by cold pressing followed by microwave sintering. Magnetic and mechanical properties of the green compact as well as sintered samples were measured. Coercivity, permeability, resistivity, elastic modulus and transverse rupture strength values in dependence on MgO content were investigated. The influence of MgO content ratio on properties was different in the case of as pressed green samples in comparison to sintered bodies. Microstructure formation and its influence on mechanical and magnetic properties are discussed. The coercivity of the green compacts with 1-5 wt% of MgO exhibits approximately 460 A/m and after sintering decreases to approximately 290 A/m. The real part of complex permeability at the frequency of 100 kHz exhibits a maximum for 2 wt% of MgO in green compacts, while for 10 wt% in sintered samples. It was observed that increase of the content of MgO causes decrease of the permeability. Properties of the sintered composite are related to formation of magnesium ferrite as well as volume distribution of residual MgO in dependence on initial MgO ratio.
EN
Soft magnetic composite materials play an important role in nowadays industry, replacing the traditional materials such as electrical steels and soft ferrites, especially at medium and higher frequency applications. The material can be tailored for a specific application by changing the composition of the material and by adaptation of the fabrication process. The aim of this work was to investigate the morphology, phase composition and magnetic properties of soft magnetic composite materials with various magnetic content to minimize the total magnetic losses. The prepared sample series was based on the mixture of two different ferromagnets Vitrovac 6155 and Somaloy 700 without addition of insulating material. The samples were prepared by conventional powder metallurgy with particular fraction of Vitrovac in the form of a ring for magnetic measurements in AC fields and electric resistivity measurements. The samples with 5 wt% and 20 wt% fractions of Vitrovac exhibit lower values of total losses in comparison with Somaloy heat treated at 530°C.
EN
We have investigated soft magnetic composite materials to better understand the influence of binder (resin) content on the DC magnetic properties and the complex permeability. Soft magnetic composite samples were composed from NiFe powder with phenol formaldehyde resin (ATM). Ferromagnetic magnetic powder for ring-shaped samples was obtained by milling of small pieces cut of NiFe sheets. The obtained powder was annealed to partially remove structural defects. The prepared powder was mixed with phenol-formaldehyde resin in different vol.%. The mixtures were pressed into the ring-shape samples. Complex permeability and DC magnetic properties (initial magnetization curves, anhysteretic curves and hysteresis loops) were measured. Higher inner demagnetizing fields in the resin containing samples were responsible for higher coercivity and hysteresis losses, but the permeability was stable up to much higher frequencies, compared to the sample without the resin.
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