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Combustion synthesis and luminescent properties of green-emitting phosphor (Sr, Zn) Al2O4: Eu2+, B3+ for white light emitting diodes (WLED)

100%
Yao S.-S., Li Y.-Y., Chen D.-H., Tang W.-J., Peng Y.-H.
Open Physics
|
2009
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vol. 7
|
issue 1
96-101
EN
In this study, the phosphors (Sr1−x , Znx)0.9(Al2−y , By)O4 doped 10 mol % Eu2+, were prepared by combustion method as the fluorescent material for white light emitting diodes (WLEDs), performing as a light source. The luminescent properties were investigated by changing the combustion temperature, the boron concentration, and the ratio of Sr to Zn. The luminescence, crystallinity and particle morphology were investigated by using a luminescence spectrometer, X-ray diffractometer (XRD) and transmission electron microscopy (TEM), respectively. The highest intensity of Sr0.9(Al2−y , By)O4: Eu0.12+ phosphor was achieved when the combustion temperature was 600° and the concentration of B3+ was 8 mol % of the aluminate. A new blue emission was observed when the high Zn concentration (x ⩾ 0.8), and this blue emission disappeared with the Zn concentration became lower than 0.8. The combustion method synthesized phosphor (Sr0.6, Zn0.4)0.9(Al1.92, B0.08)O4: Eu0.12+ showed 3.3 times improved emission intensity compared with that of the Sr0.9(Al1.92, B0.08)O4:Eu0.12+ phosphor under λex = 390 nm.
2
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Luminescence Properties of CaAl₂O₄:Eu³⁺, Gd³⁺ Phosphors Synthesized by Combustion Synthesis Method

100%
Verma N., Singh K., Marí B., Mollar M., Jindal J.
Acta Physica Polonica A
|
2017
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vol. 132
|
issue 4
1261-1264
EN
CaAl₂O₄:Eu³⁺ (1 mol.%) co-doped with varying concentration of Gd³⁺ (1, 2, 5, and 10 mol.%) were prepared by combustion synthesis method at 600°C and further annealed at 1000°C. All the compositions were investigated for their structural and photoluminescence properties. It was observed that both states of europium i.e. Eu³⁺ and Eu²⁺ were present and ratio of these states changes on heating at 1000°C. The materials synthesized at 600°C showed high intense peak around 440 nm due to presence of Eu²⁺ and less intense peaks in the red region which were due to presence of Eu³⁺. On annealing the compounds at 1000°C, intensity of peak around 440 nm decreases and intensity of peaks in the red region increases significantly. The ⁵D₀ → ⁷F₃ transition due to Eu³⁺ at 657 nm appears as the highest intensity peak. All co-doped samples annealed at 1000°C showed the higher intensity than the mono doped sample which is due to energy transfer from the Gd³⁺ to Eu³⁺. The second rare-earth ion (Gd³⁺) acts as sensitizer and enhances the photoluminescence intensity. The X-ray diffraction spectra reveal the monoclinic phase of CaAl₂O₄ in all the samples which showed that Eu³⁺ and Gd³⁺ do not change the crystalline structure of calcium aluminate.
3
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Luminescent properties of Li2 (Ca0.99, Eu0.01) SiO4: B3+ particles as a potential bluish green phosphor for ultraviolet light-emitting diodes

100%
Yao S., Chen D.
Open Physics
|
2007
|
vol. 5
|
issue 4
558-569
EN
In our study, the 1% mol Eu2+ doped Li2CaSiO4: B3+ phosphors were prepared by the combustion method as fluorescent material for ultraviolet, light-emitting diodes (UV-LEDs) used as a light source. The properties of Li2 (Ca0.99, Eu0.01) SiO4: B3+ phosphors with urea concentration, doping boric acid and a series of initiating combustion temperature were investigated. The crystallization and particle sizes of Li2 (Ca0.99, Eu0.01) SiO4: B3+ has been investigated by using powder X-ray diffraction (XRD) and transmission electron microscopy (TEM). Luminescence measurements showed that the phosphors can be efficiently excited by UV to the visible region, and exhibited bluish green light with a peak of 480 nm. The results showed that the boric acid was effective in improving the luminescence intensity of Li2 (Ca0.99, Eu0.01) SiO4: B3+ and the optimum molar ratio of boric acid to calcium nitrate was about 0.06. The optimized phosphors Li2 (Ca0.99, Eu0.01) SiO4: B0.063+ showed 180% improved emission intensity compared with that of the Li2 (Ca0.99, Eu0.01) SiO4 phosphors under ultraviolet (λex =287 nm) excitation.
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