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Synthesis and Catalytic Properties of Iron Oxides in the Reaction of Low-Temperature Ozone Decomposition

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Rakitskaya T., Truba A., Ennan A., Baumer V., Volkova V.
Acta Physica Polonica A
|
2018
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vol. 133
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issue 4
1079-1083
EN
Two sets of iron oxide samples were synthesized applying different iron(III) precursors (FeCl₃ and Fe₂(SO₄)₃) and calcination temperature (200, 300, and 500°C). The samples were characterized by powder X-ray analysis and the Fourier transform infrared spectroscopy. Depending on the synthesis conditions, samples of iron oxides with different phase composition were obtained: polyphase (α -Fe₂O₃, γ -Fe₂O₃, Fe₃O₄, and α -FeO(OH)) and monophase (γ -Fe₂O₃ or α -Fe₂O₃) ones. For the samples of homogeneous composition, it has been found that the activity of γ -Fe₂O₃ in the reaction of ozone decomposition at ozone concentration in gaseous phase of 1 mg/m³ is much higher than the activity of α -Fe₂O₃.
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Ozone decomposition on ZnO catalysts obtained from different precursors

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Milenova K. I., Nikolov P. M., Kasabova N. A., Avramova I. A.
Polish Journal of Chemical Technology
|
2014
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vol. 16
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issue 4
55-59
EN
Kinetic investigations for ozone conversion on three different series of zinc oxide catalysts, containing pure ZnO and doped with Mn or Cu one with dopant content less than 1 wt.% were carried out. The different samples were obtained from carbonate, nitrate and acetate precursors. The as prepared catalysts were characterized by AAS, XRD, IR, EPR and BET methods. The mean size of the crystallites determined by XRD data is in the range 27÷68 nm. The presence of Mn2+ and Cu2+ ions into the ZnO matrix was established by EPR. The ozone decomposition was investigated for 30÷75°C temperature range. The zinc carbonate precursor samples show highest activity, while the nitrate precursor ones show lowest activity toward reaction decomposition of ozone in the whole temperature range. At 75°C two of the catalyst, obtained from carbonate precursor - ZnO and CuZnO show 100% conversion.
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