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  1. 1 Nukleonika

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  1. 1 2015

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  1. 1 Fadeeva V. I.

  2. 1 Jartych E.

  3. 1 Kubalova L. M.

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X-ray diffraction and Mössbauer spectroscopy studies of a mechanosynthesized Fe75B25alloy

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Jartych E., Kubalova L. M., Fadeeva V. I.
Nukleonika
|
2015
|
vol. 60
|
issue 1
43-46
EN
In this work, the process of formation of metastable phases was investigated for the Fe75B25 composition. Mechanical synthesis was performed in a MAPF-2M high-energy planetary ball mill under an argon atmosphere. X-ray diffraction (XRD), differential scanning calorimetry (DSC), and Mössbauer spectroscopy (MS) were applied to recognize the phases. After 6 h of milling, the material consisted of two phases, that is, metastable tetragonal t-Fe2B and amorphous phases. During further thermal processing, the metastable phase was transformed into the stable Fe2B phase.
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