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Synthesis and characteristics of titanium silicalite TS-1, Ti-Beta and Ti-MWW catalysts

100%
Wróblewska A., Fajdek A., Milchert E.
Polish Journal of Chemical Technology
|
2009
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vol. 11
|
issue 1
64-71
EN
The synthesis methods of the following titanium-silicalite catalysts: TS-1, Ti-Beta and Ti-MWW were presented. The results of the analyses of the catalysts by XRD, SEM and IR, UV-vis methods were also shown. A brief description of the catalytic performances of these catalysts in the oxidation process of olefins, alkenes, alcohols and aromatic compounds was presented.
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The new method of 1,2-epoxy-3-butanol production over titanium silicalite catalysts

88%
Wajzberg J., Wróblewska A.
Polish Journal of Chemical Technology
|
2007
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vol. 9
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issue 2
49-52
EN
The results of 1-butene-3-ol (1B3O) epoxidation over the titanium silicalite catalysts: TS-1, Ti-Beta, Ti-MCM-41 has been presented. The optimal parameters obtained for the individual catalyst were compared. The main functions describing the process were: the selectivity of transformation to 1,2-epoxy-3-butanol (1,2E3B) in relation to 1B3O consumed, the conversions of 1B3O and hydrogen peroxide and the selectivity of the transformation to organic compounds in relation to the H2O2 consumed. The main product of the epoxidation process was 1,2-epoksy-3-butanol, the chemical compounds having a lot of applications.
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