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Position of Fe ions in MgO crystalline structure

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Szczerba J., Prorok R., Stoch P., Śnieżek E., Jastrzębska I.
Nukleonika
|
2015
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vol. 60
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issue 1
143-145
EN
Magnesium oxide (MgO) is one of the most important raw materials in many branches of industry. Magnesium oxide is a popular refractory raw material because of its high refractoriness and high resistance to basic slags and environment. In many cases, use of MgO is limited by its properties, especially the presence of secondary phases like iron oxides. The amount and distribution of iron oxides can strongly influence the technological properties of MgO and depend on the manufacturing method, particularly the heat-treatment process. The aim of the study was to evaluate the influence of the heat-treatment process on amount and distribution of iron ions in a magnesium oxide lattice. The 57Fe Mössbauer effect measurements of fused and sintered magnesium oxide samples doped by the iron oxide were conducted. Investigation reveals in both cases the presence of Fe2+ as well as Fe3+ ions. Fe2+ ions occupy Mg2+ octahedral sites in the MgO lattice, whereas the Fe3+ ions are located in highly distorted octahedral coordination. The amount of Fe2+ varies from around 66% for fused samples to 30% for sintered samples.
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Preparation and properties of porous carbon material containing magnesium oxide

100%
Przepiórski J., Czyżewski A., Kapica J., de la Casa-Lillo M.
Polish Journal of Chemical Technology
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2011
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vol. 13
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issue 4
42-46
EN
Porous carbons loaded with magnesium oxide were prepared through one-step process. Poly(ethylene terephthalate) and natural magnesite were used as carbon source and MgO precursor, respectively. An impact of a temperature and relative amounts of raw components used for preparations on the textural parameters of resulting hybrid materials is presented and discussed. As found, pore structure parameters tend to decrease along with MgO loading and temperature used during preparation process. Micropore area is the parameter being reduced primarily.
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