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Microwave Absorption Study on (Bi,Pb)-Sr-Ca-Cu-O Granular Superconductors

100%
Jurga W., Piekara-Sady L., Gazda M.
Acta Physica Polonica A
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2008
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vol. 114
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issue 1
253-256
EN
(Bi,Pb)-Sr-Ca-Cu-O is considered as a system of 2201, 2212 and 2223 superconductors embedded in the insulating matrix. The size of the grains depends on the time of recrystallization. These types of ceramics exhibit a two-step transition to superconducting state. Because electrical properties depend among other on the Josephson coupling between grains, the magnetically modulated microwave absorption study was undertaken. Magnetically modulated microwave absorption signal was observed to arise just as temperature had been lowered below T₁. The shape of this signal was studied to recognize the second temperature T₂. Some strong oscillations appear on magnetically modulated microwave absorption at lower temperatures, which might be related to local percolation breakdown in superconducting network.
2
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Superconducting Regions and Kondo Effect of MgB_2 Formed by Implantation of Magnesium Ions into Boron Substrate

64%
Trybuła Z., Kempiński W., Andrzejewski B., Piekara-Sady L., Kaszyński J., Trybuła M., Piekoszewski J., Stanisławski J., Barlak M., Richter E.
Acta Physica Polonica A
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2006
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vol. 109
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issue 4-5
657-660
EN
The results of investigation of the polycrystalline boron implanted by magnesium and argon plasma pulse treatment are presented. The four-probe electric conductivity measurements and magnetically modulated microwave absorption showed the presence of superconducting islands below the temperature of 25 K. Below T=23 K we detected the Kondo effect, a logarithmic increase in the resistivity as the temperature is lowered, due to iron impurity.
3
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The Evolution of Superconducting Phase MgB_x

64%
Łoś S., Kempiński W., Piekara-Sady L., Andrzejewski B., Jurga W., Kaszyńska K., Piekoszewski J., Werner Z., Barlak M.
Acta Physica Polonica A
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2008
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vol. 114
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issue 1
179-184
EN
Thin layers of MgB_x were studied in order to define evolution of superconducting phase after Mg ions implantation into boron substrate. Three fluencies of energies 140, 80, and 40 keV were used to establish proper stoichiometry to synthesize homogeneous MgB_2 film. Additionally, the annealing processes were carried out at temperatures 400, 500, and 600°C in a furnace in an atmosphere of flowing Ar-4%H_2 gas mixture. The quality of the superconducting material was examined by magnetically modulated microwave absorption, and magnetic and resistivity measurements. The results showed that T_c becomes higher with increasing annealing temperature. However, the fraction of superconducting phase decreases, due to partial evaporation of Mg ions and their deeper migration into boron substrate.
4
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Formation of Superconducting Regions of MgB_2 by Implantation of Boron Ions into Magnesium Substrate

52%
Trybuła Z., Kempiński W., Andrzejewski B., Piekara-Sady L., Kaszyński J., Piekoszewski J., Werner Z., Richter E., Prokert F., Stanisławski J., Barlak M.
Acta Physica Polonica A
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2005
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vol. 108
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issue 1
165-170
EN
The results of investigation of the MgB_2 inter-metallic compound with the use of boron ions implantation and plasma pulse treatment are presented. The samples were characterized by: four-probe electric conductivity measurements, magnetically modulated microwave absorption, and magnetic measurements. For hydrogen and argon pulsed plasma treatment the samples with T_c ranging from 10 K to 32 K were obtained. The superconducting phase does not form a continuous layer since the resistivity does not fall down to zero. Apparently, separate islands of superconducting phase are connected through metallic Mg paths. All samples are still below the percolation threshold.
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