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Sensitive and fast determination of papaverine by adsorptive stripping voltammetry on renewable mercury film electrode

100%
Piech R., Paczosa-Bator B.
Open Chemistry
|
2013
|
vol. 11
|
issue 5
736-741
EN
The renewable mercury film electrode, applied for the determination of papaverine traces using differential pulse adsorptive stripping voltammetry (DP AdSV) is presented. The calibration graph obtained for papaverine is linear from 1.25 nM (0.42 µg L−1) to 95 nM (32.2 µg L−1) for a preconcentration time of 60 s, with correlation coefficient of 0.998. For the renewable mercury electrode (Hg(Ag)FE) with a surface area of 9.1 mm2 the detection limit for a preconcentration time of 60 s is 0.7 nM (0.24 µg L−1). The repeatability of the method at a concentration level of the analyte as low as 17 µg L−1, expressed as RSD is 3.3% (n=5). The proposed method was successfully applied and validated by studying the recovery of papaverine from drugs, urine and synthetic solution. [...]
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The determination of molybdenum in selected mushrooms by stripping voltammetry

81%
Piech R., Niewiara E., Paczosa-Bator B., Szlósarczyk M.
Open Chemistry
|
2011
|
vol. 9
|
issue 2
352-356
EN
The highly sensitive method of adsorptive stripping voltammetry (AdSV), with differential pulse steps, was performed at a mercury film electrode and has been applied here for the determination of trace molybdenum content in selected wild mushrooms. Fruiting body caps of 12 selected macrofungi species from Basidiomycetes have been investigated. Molybdenum content of investigated samples was determined in the range of 0.006 to 0.38 mg kg−1 of dry matter. The highest value of molybdenum content was found in Leccinum rufum and the lowest in Lactarius deliciosus.
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