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EN
In the work the thermal behaviour of the magnetic nanoparticles modified with polysaccharide dextran of different weight ratios to the magnetite Fe_3O_4 was investigated using thermoanalytical methods - differential scanning calorimetry and thermogravimetric analysis. The adsorption of dextran on the magnetic nanoparticles was confirmed and the influence of the dextran amount in the modified magnetic fluid on the thermal decomposition of the complex system was studied. The results showed that magnetite catalyzed the thermal decomposition of dextran, the adsorbed dextran showed lower initial decomposition temperatures in comparison with the free one.
EN
Magnetic nanoparticles used in biomedicine have to be biocompatible, which can be achieved by the modification of the magnetic particle surface with an appropriate biocompatible substance. In the work protein bovine serum albumin (BSA) was chosen to modify the surface of magnetic nanoparticles. The BSA-coated magnetic nanoparticles with different input weight ratios of BSA to the magnetite Fe_3O_4 were prepared and thermally characterized using thermogravimetric and differential scanning calorimetric analysis. The adsorption of BSA on the magnetic nanoparticles in wide range of concentration was confirmed. The activation energies of the thermal decomposition of the complex system were estimated.
EN
This paper deals with the preparation and complex characterization of magnetite nanoparticles (MNPs), stabilized with sodium oleate (SO), by the routine methods such as infrared spectroscopy (FTIR), magnetic measurements, scanning electron microscopy (SEM) and dynamic light scattering (DLS). The FTIR spectra showed that SO molecules were linked to MNPs through chemical bonding. Magnetic measurements proved that the MNPs are superparamagnetic in nature. Four different methods were used to determine the size and size distribution of the MNPs: SEM, DLS, differential centrifugal sedimentation (DCS) and magnetic measurements. SEM analysis showed a relatively narrow size distribution of roughly spherical MNPs with a mean diameter of 61 nm. DLS analysis confirmed monodispersed MNPs production with hydrodynamic diameter of 75 nm. The size distribution determined by DCS was found to be 69 nm. Finally, the calculated magnetic core diameter obtained from magnetization curve was 10 nm. The obtained results demonstrate that SO coated MNPs fulfil the requirements for a useful drug delivery system.
EN
In this work the interaction of lysozyme fibrils with magnetic particles has been studied by atomic force microscopy. The experiments were carried out for a better understanding of the binding process of such complex soft matter systems. The obtained results show that interaction between lysozyme fibrils and magnetic particles starts immediately after mixing them together. Moreover, the samples remain stable in duration of several days after preparation.
EN
The aim of the presented work was to investigate the stability of biocompatible magnetic fluid, i.e. water-based magnetic fluid containing magnetite nanoparticles stabilized by surfactant sodium oleate and modified by bovine serum albumin (BSA) after electron irradiation. Samples with the same concentration of Fe_{3}O_{4} but different mass ratio BSA/Fe_{3}O_{4} (w/w=0.25, 1.0 and 2.5) were studied. The electron irradiation caused about 10% reduction of the saturation magnetization in the samples with w/w BSA/Fe_{3}O_{4} ratio of 0.25 and less than 5% in the samples with w/w BSA/Fe_{3}O_{4} ratio of 1 and 2.5.
6
68%
EN
An important feature of lyotropic liquid crystals is the self-assembly of the amphiphilic molecules as supermolecular structures. We have studied the formation of nematic liquid crystal phase in solutions containing lysozyme amyloid fibrils and magnetic nanoparticles using oscilloscopic method. Interaction of fibrils with magnetic nanoparticles under the external magnetic field resulted in fibril re-arrangement. The analysis of the obtained results suggests that the decrease in conductivity of solutions in presence of magnetic field is due to decrease of the ion mobility caused by re-arrangement of structures in the solution. The obtained results allow determination of the optimum ratio of the components which can lead to preparation of solutions with a more ordered structure in presence of magnetic field.
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