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Characterization of Coating Formed on Pure Zirconium by MAO in Yttrium Acetate Tetrahydrate Containing Electrolyte

100%
Cengiz S., Yazici M., Gencer Y., Tarakci M.
Acta Physica Polonica A
|
2015
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vol. 127
|
issue 4
1320-1325
EN
In this study, oxide coatings were produced on pure zirconium by micro arc oxidation method in the electrolytes containing sodium silicate and different amounts of yttrium acetate tetrahydrate (1-4 g/l) for the same coating duration of 1 h. The surface roughness, microstructure, phase content and chemical composition of the coatings were characterized by using scanning electron microscopy, profilometry and X-Ray diffractometry. It was found that the surfaces of coatings on zirconium consist of monoclinic-ZrO₂, tetragonal-ZrO₂ phases. The coating thickness decreases with addition of yttrium acetate tetrahydrate while it does not change significantly with the increase of its amount. The clustered equiaxed features were formed on the surfaces of the coatings. As the amount of yttrium acetate tetrahydrate in the electrolyte solution increased, the coating/substrate interface smoothened. Two main regions of the coating, the outer dense region (I) and the porous inner region (II), became significant with addition of YAT into the electrolyte.
2
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Oxide Based Ceramic Coating on Al-4Cu Alloy by Microarc Oxidation

88%
Cengiz S., Tarakci M., Gencer Y., Devecili A., Azakli Y.
Acta Physica Polonica A
|
2013
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vol. 123
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issue 2
445-448
EN
In this study the Al-Cu aluminum alloy with 4 wt% Cu was prepared under controlled atmosphere and coated by microarc oxidation technique for the durations of 40, 80, and 120 min. The phase composition, surface roughness and hardness of the coating were characterized by X-ray diffraction, scanning electron microscopy, profilometry. The outer region contains larger sized porosities while fine porosities were formed in the inner dense region of the coating. The longer coating duration resulted in dense inner region with finely distributed α-Al_2O_3 precipitates. The presence of Cu in the outer region is not significant while the presence of Si in inner region was lower than in the outer region. Mullite and γ-Al_2O_3 phases were formed for 40 min and α-Al_2O_3 phase was additionally formed for 80 min and 120 min coating time. The coating thickness increased from 38 μm (40 min) to 115 μm (120 min) while the surface roughness (R_{a}) increased from 5 μm (40 min) to 9 μm (120 min).
3
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Effects of the Addition of Calcium Acetate into Silicate-Based Electrolytes on the Properties of MAO Coatings Produced on Zirconium

76%
Cengiz S., Azakli Y., Yazici M., Gayretli B., Gencer Y., Tarakci M.
Acta Physica Polonica A
|
2016
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vol. 129
|
issue 4
504-508
EN
Zirconium (Zr) is a potential implant material due to its excellent biocompatibility and low elastic modulus for biomedical applications. Its poor bioactivity, however, limits its use as biomaterials. In this study, microarc oxidation which is a plasma-electrochemical based process was applied to produce oxide coatings on pure zirconium. The coating processes were conducted in different electrolytes containing sodium silicate and varying amounts of calcium acetate tetrahydrate (CA) for 30 min to investigate the effect of the introduction of CA into the electrolyte solution on the morphology and chemical composition of the fabricated coatings. It was found that the coatings consisted of monoclinic-ZrO₂ and tetragonal-ZrO₂ phases. The amount of the tetragonal-ZrO₂ phase increased with the increasing CA concentration in the electrolyte. The coating thickness and surface roughness showed a tendency to increase with the increasing CA concentration in the electrolyte. It was observed that the vicinity of plasma channels were Zr-rich, while their surroundings were rich in Si and Ca elements. The outer region of the coating was denser compared to inner region consisting of Zr-rich porous structure.
4
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Effects of the Addition of Calcium Acetate into Silicate-Based Electrolytes on the Properties of MAO Coatings Produced on Zirconium (Acta Physica Polonica A 129, 504 (2016), ERRATUM)

76%
Cengiz S., Azakli Y., Yazici M., Gayretli B., Gencer Y., Tarakci M.
Acta Physica Polonica A
|
2017
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vol. 132
|
issue 4
1436
EN
The article was originally published on October 2014. In this paper "calcium acetate monohydrate" was used in electrolyte solution, however by mistake authors had written the name of the chemical as "calcium acetate tetrahydrate". The authors apologize for their error.
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