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  1. 1 Open Chemistry

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  1. 1 2010

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  1. 1 Kelly B.

  2. 1 Kramer J.

  3. 1 Manivannan V.

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Synthesis of MSn(OH)6 (where M = Mg, Ca, Zn, Mn, or Cu) materials at room temperature

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Kramer J., Kelly B., Manivannan V.
Open Chemistry
|
2010
|
vol. 8
|
issue 1
65-69
EN
Applying a metathesis approach (MCl2·xH2O+Na2SnO3·xH2O→MSn(OH)6+NaCl+xH2O), Schoenfliesite-type materials with general formula MSn(OH)6 (where M=Ca, Cu, Mg, Mn or Zn) were synthesized at room-temperature. The high lattice-energy of the by-product alkali halide NaCl drives the reaction in the forward direction leading to the formation of the desired materials. The materials synthesized were characterized by powder X-ray diffraction (XRD) and scanning electron microscopy (SEM) to elucidate structural and micro structural features. [...]
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