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1
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Electrical Conductivity, Viscosity and Thermal Properties of TEGDME-Based Composite Electrolytes for Lithium-Air Batteries

100%
Kartal M., Alp A., Akbulut H.
Acta Physica Polonica A
|
2016
|
vol. 129
|
issue 4
816-818
EN
Some important properties of the electrolytes used in Li-air batteries were investigated. Electrolyte composed of a solution of 1 M LiPF₆ in tetra ethylene glycol dimethyl ether (TEGDME) was reinforced with SiO₂, Al₂O₃, poly(ethylene) oxide (PEO) and tris (pentafluorophenyl) borane (TPFPB) additives. The effects of these reinforcements on conductivity, viscosity and thermal stability were investigated. Electrical conductivity tests were carried out using a multiparameter meter. Viscosity tests were performed in a viscometer using tuning-fork vibration method. Thermal stability of the electrolytes was tested by both TG and DSC.
2
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Pulse Electrodeposition of Copper-Zinc Coatings from an Alkaline Bath

100%
Kartal M., Alp A., Akbulut H.
Acta Physica Polonica A
|
2017
|
vol. 132
|
issue 3
801-803
EN
A copper-zinc bath containing EDTA was used for deposition of multi-functional copper-zinc coatings. Copper substrates were used for pulse electrodeposition of copper-zinc coating. Microhardness and wear resistance of copper-zinc coatings has been studied. The films were characterized by scanning electron microscopy and X-ray diffraction. EDS and EDS-dot mapping were also performed to analyse the amount and the distribution of Cu-Zn atoms.
3
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Si/Mo/MWCNT Nanocomposites for Lithium Ion Battery Applications

88%
Cetinkaya T., Uysal M., Tokur M., Kartal M., Akbulut H.
Acta Physica Polonica A
|
2015
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vol. 127
|
issue 4
1048-1051
EN
In this study, silicon/multi-wall carbon nanotube (Si/MWCNT) and silicon/molybdenum/multi-wall carbon nanotube (Si/Mo/MWCNT) composites were produced by high speed planetary ball milling. Produced Si/MWCNT composite containing 50 wt.% Si and 50 wt.% MWCNT and dispersingdifferent amount of molybdenum nanopowders (1 wt.%, 3 wt.% and 5 wt.%) Si/Mo/MWCNT composites were produced by high speed planetary ball milling. Surface morphology of produced composite electrodes was characterized using scanning electron microscopy (SEM) and EDS dot-map analyze was performed to investigate dispersion of MWCNT and molybdenum powders in the composite structure. X-ray diffraction (XRD) technique was carried out to investigate structure of produced Si/Mo/MWCNT composites. Electrochemical performance of the electrodes were tested between 50 mV and 1.5 V in CR2016 test cell.
4
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The Effect of Inorganic Nano Powder Additives in TEGDME for Lithium Air Batteries

88%
Kartal M., Uysal M., Cetinkaya T., Alp A., Akbulut H.
Acta Physica Polonica A
|
2015
|
vol. 127
|
issue 4
1016-1018
EN
SiO₂ and Al₂O₃ nano fillers were added to an electrolyte composed of a solution 1 M LiPF₆ in tetra ethylene glycol dimethyl ether (TEGDME) and the effects of these nano powders on capacity and cycling performances were investigated. Galvanostatic charge/discharge (GC) measurements were performed in the assembled Li-air cells by using the nanocomposite electrolytes. The discharge capacities of these cells were cyclically tested by a battery tester at a constant current in the voltage range between 2.15 V and 4.25 V. Discharge products of nanocomposite electrolytes were characterized by SEM and XRD spectroscopies. The electrochemical results demonstrated that Al₂O₃ reinforced electrolyte showed higher discharge capacity and cyclability than those of SiO₂ reinforced electrolyte.
5
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Preparation and Characterization of Copper Powders with Sn Coating by the Electroless Plating

64%
Uysal M., Cetinkaya T., Gul H., Kartal M., Algul H., Tokur M., Alp A., Akbulut H.
Acta Physica Polonica A
|
2015
|
vol. 127
|
issue 4
1106-1108
EN
In this work, Sn-Cu composite powders were produced using an electroless process. The tin content on the surface of copper powders was varied by using different concentrations of SnSO₄ in the plating bath. The surface morphology of the produced Sn-Cu composite powders was characterized using scanning electron microscopy (SEM). Energy dispersive spectroscopy (EDS) was used to determine the elemental surface composition of the composites. X-ray diffraction (XRD) analysis was performed to investigate the structure of the Sn-Cu composite powders. The electrochemical performance of Sn-Cu nanocomposites was studied by charge/discharge tests.
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