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Superionic Phase Transition in Rb_{4}LiH_{3}(SeO_{4})_{4} Single Crystals

100%
Połomska M., Hilczer B., Wolak J., Pietraszko A.
Acta Physica Polonica A
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1994
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vol. 85
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issue 5
825-833
EN
Derivatographic, dielectric and complex impedance studies of Rb_{4}LiH_{3}(SeO_{4})_{4} crystals revealed a superionic phase transition at T_{s} ≈ 448 K. The bulk conductivity rises from 10^{-6} to 10^{-4} (Ωm)^{-1} at T_{s}, and the activation energy of conductivity in the direction of crystal axes a and b (where a = b for tetragonal symmetry) W_{a} = W_{b} decreases from 0.94 eV in the low temperature phase to the value of 0.27 eV at T > T_{s}. The analysis of the results of X-ray studies at room temperature and at 450 K indicates that the fast ion transport, characterized by low activation energy, is related to the delocalization of the H2 protons in the O(12)-H2-O(24) bonds linking the Se(1)O_{4} and Se(2)O_{4} tetrahedra. The "cogwheel" mechanism is suggested to be involved in the fast proton transport.
2
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Effect of Nd³⁺ Doping on Magnetic and Dielectric Properties of SrFe₁₂O₁₉ Hexaferrite Synthesized by Coprecipitation Method

88%
Hilczer A., Pasińska K., Markiewicz E., Pietraszko A., Andrzejewski B.
Acta Physica Polonica A
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2018
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vol. 133
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issue 3
669-672
EN
Magnetic and dielectric properties of hexagonal ferrites important for applications in microwave absorbers are strongly determined by the processing conditions. We studied dielectric and magnetic response of Sr_{1-x}Nd_{x}Fe₁₂O₁₉ (x=0, 0.03, 0.05, 0.07, 0.09) solid solutions obtained by coprecipitation method. The structure of the samples was controlled by X-ray diffraction and scanning electron microscope images revealed that the powder is a mixture of small nanograins and crystallites of 500 nm-1 μm in size. Nd³⁺ doping was found to result in an increase in the coercive field which we would like to relate to the domain wall pinning. The doping-induced changes are monotonous with x up to 0.07. The observed dispersion of permittivity was found to be correlated with the frequency behaviour of electric conductivity of the samples.
3
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X-Ray Characterization of GaAs:Zn Gas-transport Grown Whiskers Using Conventional and Synchrotron Sources

64%
Paszkowicz W., Górecka J., Domagała J., Dmitruk N., Varshava S. S., Härtwig J., Ohler M., Pietraszko A.
Acta Physica Polonica A
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1997
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vol. 91
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issue 5
997-1002
EN
GaAs:Zn whiskers grown by the gas-transport method are characterized by diffraction methods using white and monochromatic radiation. The methods applied include the white-beam topography at ESRF synchrotron source and Laue patterns, 4-circle Bond diffractometry and high-resolution diffractometry at conventional X-ray sources. The results obtained concern the growth morphology and defect structure. It is found that GaAs:Zn whiskers grown by the described method have the form of long needles and blades of the morphologies represented by growth direction and largest lateral face ⟨112⟩{111} and ⟨111⟩{112}, respectively, with a single exception of a blade of uncommon morphology ⟨111⟩{110}.
4
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Electron Microscopy and X-ray Structural Investigations of Incommensurate Spin-Ladder Sr_{4.1}Ca_{4.7}Bi_{0.3}Cu_{17}O_{29} Single Crystals

64%
Dłużewski P., Pietraszko A., Kozłowski M., Szczepańska A., Górecka J., Baran M., Leonyuk L., Babonas G.-J., Lebedev O., Szymczak R.
Acta Physica Polonica A
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2000
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vol. 98
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issue 6
729-737
EN
Transmission electron microscopy and X-ray diffraction proved chain ladder incommensurate single crystal structure of investigated samples. The incommensurate ratio was determined from the X-ray and electron diffraction being equal to 0.704. Diffuse scattering intensities localised on the planes perpendicular to the c*-axis and passing through the spots originating from the periodicity of chain sublattice were detected. High-angle grain boundary or twinning formed by rotation of 33.3° around [100] direction was observed. High-resolution electron microscopy images revealed the stacking faults in ac planes.
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